Magnetism of iron-containing MCM-41 spheres

被引:31
作者
Liu, SQ [1 ]
Wang, Q
Van Der Voort, P
Cool, P
Vansant, EF
Jiang, MH
机构
[1] Jinan Univ, Sch Mat Sci & Engn, Jinan 250022, Shandong, Peoples R China
[2] Univ Instelling Antwerp, Lab Adsorpt & Catalysis, B-2610 Antwerp, Belgium
[3] Shandong Univ, Sch Mat Sci & Engn, Jinan 250100, Shandong, Peoples R China
关键词
MCM-41; spheres; iron-loading; magnetism; pyrolysis;
D O I
10.1016/j.jmmm.2004.02.019
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Iron species were loaded into the mesopores of MCM-41 spheres by incipient wetness impregnation procedure with Fe(ACAC)(3) as the precursor. The magnetism of the samples was studied by vibrating sample magnetometer (VSM), diffuse reflectance ultraviolet-visible (DRUV-vis) spectra and Mossbauer spectra. The results show that the magnetic behavior of the iron-loaded MCM-41 spheres depends on the content of iron loading, valence, and coordination state of iron ions, testing temperature and the atmosphere for the pyrolysis of the iron precursor. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:31 / 36
页数:6
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