Synthesis and properties of new fullerene C60 derivatives, containing acetonide and polyol fragments

被引：5

作者：

Gilmutdinova, Alina A. ^{[1
]}

Gubskaya, Valentina P. ^{[1
]}

Fazleeva, Guzel M. ^{[1
]}

Latypov, Shamil K. ^{[1
]}

Zhelonkina, Tatyana A. ^{[1
]}

Sharafutdinova, Dilara R. ^{[1
]}

Nuretdinov, Ildus A. ^{[1
]}

Sinyashin, Oleg G. ^{[1
]}

机构：

[1] RAS, Kazan Sci Ctr, AE Arbuzov Organ & Phys Chem Inst, Kazan 420088, Russia

来源：

TETRAHEDRON | 2014年 / 70卷 / 35期

基金：

俄罗斯基础研究基金会;

关键词：

Hexa-methanofullerenes; Acetonide protection; Bingel-Hirsch reaction; Water-soluble polyol methanofullerenes; OCTAHEDRAL ADDITION PATTERN; EFFICIENT SYNTHESIS; BUILDING-BLOCKS; WATER; C60;

D O I：

10.1016/j.tet.2014.06.009

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

New mono- and hexa-methanofullerenes containing different number of acetonide groups are synthesized and characterized. Removing the acetonide protection leads to new chromatographically pure water-soluble polyol methanofullerenes with essentially quantitative yields. (C) 2014 Elsevier Ltd. All rights reserved.

引用

页码：5947 / 5953

页数：7

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