A rapid and efficient synthesis of symmetrical disulfides under microwave irradiation conditions

被引：34
|
作者：
Wang, JX
Gao, LJ
Huang, DF
机构：
[1] NW Normal Univ, Dept Chem, Inst Chem, Lanzhou 730070, Peoples R China
[2] Ningxia Univ, Dept Chem, Yinchuan 75000, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2002年 / 32卷 / 07期
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1081/SCC-120003143
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A rapid and general method for the synthesis of symmetrical disulfides involves reaction of sulfur with sodium hydroxide under PTC-microwave irradiation condition to give sodium disulfide, which reacts with alkyl halides to afford the disulfides in good to excellent isolated yields.
引用
收藏
页码：963 / 969
页数：7
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