A rapid and efficient synthesis of symmetrical disulfides under microwave irradiation conditions

被引：34
|
作者：
Wang, JX
Gao, LJ
Huang, DF
机构：
[1] NW Normal Univ, Dept Chem, Inst Chem, Lanzhou 730070, Peoples R China
[2] Ningxia Univ, Dept Chem, Yinchuan 75000, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2002年 / 32卷 / 07期
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1081/SCC-120003143
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A rapid and general method for the synthesis of symmetrical disulfides involves reaction of sulfur with sodium hydroxide under PTC-microwave irradiation condition to give sodium disulfide, which reacts with alkyl halides to afford the disulfides in good to excellent isolated yields.
引用
收藏
页码：963 / 969
页数：7
相关论文
共 50 条
  • [1] Rapid and efficient synthesis of symmetrical alkyl disulfides under phase transfer conditions
    Sonavane, Sachin U.
    Chidambaram, Mandan
    Almog, Joseph
    Sasson, Yoel
    TETRAHEDRON LETTERS, 2007, 48 (34) : 6048 - 6050
  • [2] DRY SYNTHESIS UNDER MICROWAVE IRRADIATION - A RAPID AND EFFICIENT COUPLING OF NAPHTHOLS
    VILLEMIN, D
    SAUVAGET, F
    SYNLETT, 1994, (06) : 435 - 436
  • [3] Rapid and efficient synthesis of imidazolines and bisimidazolines under microwave and ultrasonic irradiation
    Moghadam, Majid
    Mohammadpoor-Baltork, Iraj
    Mirkhani, Valiollah
    Tangestaninejad, Shahram
    Abdollahi-Alibeik, Mohammad
    Yousefi, Behrooz H.
    Kargar, Hadi
    MONATSHEFTE FUR CHEMIE, 2007, 138 (06): : 579 - 583
  • [4] A rapid and efficient synthesis of indoloquinolinone and its analogues under microwave irradiation
    Yu Jing Lu Ning Sun Zhi Shu Huang* Lian Quan Gu* School of Pharmaceutical Sciences
    ChineseChemicalLetters, 2008, (05) : 518 - 520
  • [5] Rapid and Efficient Synthesis of Imidazolines and Bisimidazolines Under Microwave and Ultrasonic Irradiation
    Majid Moghadam
    Iraj Mohammadpoor-Baltork
    Valiollah Mirkhani
    Shahram Tangestaninejad
    Mohammad Abdollahi-Alibeik
    Behrooz H. Yousefi
    Hadi Kargar
    Monatshefte für Chemie - Chemical Monthly, 2007, 138 : 579 - 583
  • [6] Rapid and efficient synthesis of 1-arylpiperazines under microwave irradiation
    Jaisinghani, HG
    Khadilkar, BM
    TETRAHEDRON LETTERS, 1997, 38 (39) : 6875 - 6876
  • [7] A rapid and efficient synthesis of indoloquinolinone and its analogues under microwave irradiation
    Lu, Yu Jing
    Sun, Ning
    Huang, Zhi Shu
    Gu, Lian Quan
    CHINESE CHEMICAL LETTERS, 2008, 19 (05) : 518 - 520
  • [8] Rapid and Efficient Synthesis of N-alkylbenzamides Under Microwave Irradiation
    Cermak, Jan K.
    Kolar, Karel
    Cirkva, Vladimir
    LETTERS IN ORGANIC CHEMISTRY, 2013, 10 (02) : 126 - 130
  • [9] Rapid and Convenient Method for the Synthesis of Symmetrical Disulfides
    Bahrami, Kiumars
    Khodaei, Mohammad M.
    Shakibaian, Vida
    Targhan, Homa
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2013, 188 (08) : 981 - 988
  • [10] A rapid and efficient synthesis of thiochroman-4-ones under microwave irradiation
    Li, JT
    Li, HY
    Li, HZ
    Xiao, LW
    JOURNAL OF CHEMICAL RESEARCH, 2004, (06) : 394 - 395
12345