Vortex-Assisted Liquid-Liquid Microextraction for Steroid Profile Analysis: Towards Sustainable Development Goals 2030

被引：0

作者：

Manaf, Normaliza Abdul ^{[1
,2
]}

Saad, Bahruddin ^{[1
,3
]}

Latiff, Aishah A. ^{[4
]}

Sibly, Suzyrman ^{[2
]}

机构：

[1] Univ Sains Malaysia, Sch Chem Sci, George Town, Malaysia

[2] Univ Sains Malaysia, Ctr Global Sustainabil Studies, George Town, Malaysia

[3] Univ Teknol Petronas, Fundamental & Appl Sci Dept, Perak, Malaysia

[4] Antidoping Lab Qatar, Doha, Qatar

来源：

UNIVERSITIES AS LIVING LABS FOR SUSTAINABLE DEVELOPMENT: SUPPORTING THE IMPLEMENTATION OF THE SUSTAINABLE DEVELOPMENT GOALS | 2020年

关键词：

Green chemistry; Microextraction; Steroid profile; LC-MS/MS; Urine analysis; Sustainable development goals; GREEN ANALYTICAL-CHEMISTRY; PHASE MICROEXTRACTION; DOPING CONTROL; CHROMATOGRAPHY; WATER; PRINCIPLES; HORMONES;

D O I：

10.1007/978-3-030-15604-6_45

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Prevention of waste is among of 12 principles in green chemistry. This study discusses about a simple, rapid and environmentally friendly method for the determination of endogenous steroid profile. Avortex assisted liquid-liquidmicroextraction (VALLME) as sample preparation followed by liquid chromatography tandem mass spectrometry (LC-MS/MS) for the determination of steroid profile in urine was identified. The proposed method fulfilled the green chemistry principle and Goal 13 in Sustainable Development Goals.

引用

页码：747 / 760

页数：14

共 44 条

[1] Quantification of endogenous steroids in human urine by gas chromatography mass spectrometry using a surrogate analyte approach [J].

Ahmadkhaniha, Reza ;

Shafiee, Abbas ;

Rastkari, Noushin ;

Khoshayand, Mohammad Reza ;

Kobarfard, Farzad .

JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2010, 878 (11-12) :845-852

[2]

Anastas P.T., 1998, Oxford University Press eBooks, P640, DOI DOI 10.1093/OSO/9780198506980.001.0001

[3]

[Anonymous], 2019, ASS BIOPH SOC VULN N

[4] SOLID-PHASE MICROEXTRACTION WITH THERMAL-DESORPTION USING FUSED-SILICA OPTICAL FIBERS [J].

ARTHUR, CL ;

PAWLISZYN, J .

ANALYTICAL CHEMISTRY, 1990, 62 (19) :2145-2148

[5] Carbon isotope ratio (δ13C) values of urinary steroids for doping control in sport [J].

Cawley, Adam T. ;

Trout, Graham J. ;

Kazlauskas, Rymantas ;

Howe, Christopher J. ;

George, Adrian V. .

STEROIDS, 2009, 74 (03) :379-392

[6] Are sub-2 μm particles best for separating small molecules? An alternative [J].

DeStefano, Joseph J. ;

Boyes, Barry E. ;

Schuster, Stephanie A. ;

Miles, William L. ;

Kirkland, Joseph J. .

JOURNAL OF CHROMATOGRAPHY A, 2014, 1368 :163-172

[7]

Donike M., 1993, Proceedings of the 10th Cologne Workshop on Dope Analysis, P69

[8] Green analytical chemistry in the determination of organic pollutants in the aquatic environment [J].

Farre, Marinella ;

Perez, Sandra ;

Goncalves, Carlos ;

Alpendurada, M. F. ;

Barcelo, Damia .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2010, 29 (11) :1347-1362

[9] The 12 principles of green analytical chemistry and the SIGNIFICANCE mnemonic of green analytical practices [J].

Galuszka, Agnieszka ;

Migaszewski, Zdzislaw ;

Namiesnik, Jacek .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2013, 50 :78-84

[10]

Gyorgy V., 2004, J MASS SPECTROM, V39, P233, DOI DOI 10.1002/JMS.606

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