Preparation of iron/graphite core-shell structured nanoparticles

被引:35
作者
David, B
Pizúrová, N
Schneeweiss, O
Bezdicka, P
Morjan, I
Alexandrescu, R
机构
[1] Acad Sci Czech Republic, Inst Phys Mat, CZ-61662 Brno, Czech Republic
[2] Acad Sci Czech Republic, Inst Inorgan Chem, CZ-25068 Rez, Czech Republic
[3] Natl Inst Lasers Plasma & Radiat Phys, R-76900 Bucharest, Romania
关键词
nanoparticles; laser-induced pyrolysis; Mossbauer spectroscopy; magnetic measurements;
D O I
10.1016/j.jallcom.2003.10.088
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The paper presents a magnetic and morphological characterization of iron- and iron-carbide-based nanopowder obtained by the laser synthesis from a sensitized gas phase mixture containing acetylene and iron pentacarbonyl vapor. The analysis was performed on the as-prepared material and the annealed material. We report here the results of TEM, XRD, Mossbauer and magnetic measurements. Phase transformations taking place during annealing when core-shell-like nanostructures appear are discussed. (C) 2004 Published by Elsevier B.V.
引用
收藏
页码:112 / 116
页数:5
相关论文
共 21 条
[1]  
ALEXANDRESCU P, 1999, J PHYS IV, V9, pPR8
[2]   Iron-oxide-based nanoparticles produced by pulsed infrared laser pyrolysis of Fe(CO)5 [J].
Alexandrescu, R ;
Morjan, I ;
Crunteanu, A ;
Cojocaru, S ;
Petcu, S ;
Teodorescu, V ;
Huisken, F ;
Kohn, B ;
Ehbrecht, M .
MATERIALS CHEMISTRY AND PHYSICS, 1998, 55 (02) :115-121
[3]  
[Anonymous], 1996, BIN ALL PHAS DIAGR
[4]   NANOCRYSTALLINE ALPHA-FE, FE3C, AND FE7C3 PRODUCED BY CO2-LASER PYROLYSIS [J].
BI, XX ;
GANGULY, B ;
HUFFMAN, GP ;
HUGGINS, FE ;
ENDO, M ;
EKLUND, PC .
JOURNAL OF MATERIALS RESEARCH, 1993, 8 (07) :1666-1674
[5]  
DERBISHIRE FJ, 1975, CARBON, V42, P111
[6]  
FIATO RA, 1987, Patent No. 4659681
[7]   Role of the catalyst particle size in the synthesis of single-wall carbon nanotubes [J].
Gorbunov, A ;
Jost, O ;
Pompe, W ;
Graff, W .
APPLIED SURFACE SCIENCE, 2002, 197 :563-567
[8]   Solid-liquid-solid growth mechanism of single-wall carbon nanotubes [J].
Gorbunov, A ;
Jost, O ;
Pompe, W ;
Graff, A .
CARBON, 2002, 40 (01) :113-118
[9]  
HAGGERTY JS, 1981, LASER INDUCED CHEM P, pCH3
[10]   Catalytic production and purification of nanotubules having fullerene-scale diameters [J].
Ivanov, V ;
Fonseca, A ;
Nagy, JB ;
Lucas, A ;
Lambin, P ;
Bernaerts, D ;
Zhang, XB .
CARBON, 1995, 33 (12) :1727-1738