Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N',N'-tetramethylmethanediamine and α,ω-alkanedithiols

被引：2
作者：
Khairullina, R. R. [1 ]
Geniyatova, A. R. [1 ]
Meshcheryakova, E. S. [1 ]
Tyumkina, T. V. [1 ]
Khalilov, L. M. [1 ]
Ibragimov, A. G. [1 ]
Dzhemilev, U. M. [1 ]
机构：
[1] Russian Acad Sci, Inst Petrochem & Catalysis, Pr Oktyabrya 141, Ufa 450075, Bashkortostan, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2017年 / 53卷 / 03期
基金：
俄罗斯基础研究基金会;
关键词：
CARBOXYLIC-ACID HYDRAZIDES; ANTIMICROBIAL ACTIVITY; N,6-DIARYL-4-METHYL-2-THIOXO-1,2,3,6-TETRAHYDROPYRIMIDINE-5-CARBOXAMIDES; H2S;
D O I：
10.1134/S1070428017030010
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient procedure has been developed for the synthesis of N,N'-(2,5-dithiaalkane-alpha,omega-diyl)bis-(N'-allylthioureas) by thiomethylation of N-substituted ureas and thioureas with alpha,omega-alkanedithiols and N,N,N',N'-tetramethylmethanediamine in the presence of cesium carbonate as catalyst.
引用
收藏
页码：315 / 321
页数：7
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