High resolution and high fields in biological solid state NMR

被引：13

作者：

Cotten, M

Soghomonian, VG

Hu, W

Cross, TA

机构：

[1] FLORIDA STATE UNIV,INST MOL BIOPHYS,NATL HIGH MAGNET FIELD LAB,TALLAHASSEE,FL 32306

[2] FLORIDA STATE UNIV,DEPT CHEM,TALLAHASSEE,FL 32306

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1997年 / 9卷 / 01期

基金：

美国国家科学基金会;

关键词：

high resolution; high fields; biological solid state NMR;

D O I：

10.1016/S0926-2040(97)00046-5

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

H-2 solid state NMR spectra of a polypeptide in an oriented membrane environment is demonstrated to have an orientational resolution of 0.3 degrees. Such data results in high resolution structural constraints. Similar spectra are demonstrated at 23.2 T using a resistive magnet at the National High Magentic Field Laboratory. (C) 1997 Elsevier Science B.V.

引用

收藏

页码：77 / 80

页数：4

相关论文

共 12 条

[1]

Andrew E.R., 1969, J MAGN RESON, V1969, P27

[2] NUCLEAR MAGNETIC RESONANCE SPECTRA FROM A CRYSTAL ROTATED AT HIGH SPEED [J].

ANDREW, ER ;

BRADBURY, A ;

EADES, RG .

NATURE, 1958, 182 (4650) :1659-1659

[3] Direct determination of a molecular torsional angle by solid-state NMR [J].

Feng, X ;

Lee, YK ;

Sandstrom, D ;

Eden, M ;

Maisel, H ;

Sebald, A ;

Levitt, MH .

CHEMICAL PHYSICS LETTERS, 1996, 257 (3-4) :314-320

[4] DEUTERIUM NMR OF VAL1...(2-H-2)ALA3...GRAMICIDIN-A IN ORIENTED DMPC BILAYERS [J].

HING, AW ;

ADAMS, SP ;

SILBERT, DF ;

NORBERG, RE .

BIOCHEMISTRY, 1990, 29 (17) :4144-4156

[5] TRYPTOPHAN DYNAMICS AND STRUCTURAL REFINEMENT IN A LIPID BILAYER ENVIRONMENT - SOLID-STATE NMR OF THE GRAMICIDIN CHANNEL [J].

HU, W ;

LAZO, ND ;

CROSS, TA .

BIOCHEMISTRY, 1995, 34 (43) :14138-14146

[6]

Ketchem RR, 1996, J BIOMOL NMR, V8, P1

[7] HIGH-RESOLUTION CONFORMATION OF GRAMICIDIN-A IN A LIPID BILAYER BY SOLID-STATE NMR [J].

KETCHEM, RR ;

HU, W ;

CROSS, TA .

SCIENCE, 1993, 261 (5127) :1457-1460

[8] Distance measurements in nucleic acids using windowless dipolar recoupling solid state NMR [J].

Mehta, MA ;

Gregory, DM ;

Kiihne, S ;

Mitchell, DJ ;

Hatcher, ME ;

Shiels, JC ;

Drobny, GP .

SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1996, 7 (03) :211-228

[9]

MOLL F, 1988, THESIS FLORIDA STATE

[10] CORRELATIONS BETWEEN FUNCTION AND DYNAMICS - TIME-SCALE COINCIDENCE FOR ION TRANSLOCATION AND MOLECULAR-DYNAMICS IN THE GRAMICIDIN CHANNEL BACKBONE [J].

NORTH, CL ;

CROSS, TA .

BIOCHEMISTRY, 1995, 34 (17) :5883-5895