A Forward Modeling Approach to High-Reliability Grain Mapping by Laboratory Diffraction Contrast Tomography (LabDCT)

被引:22
作者
Niverty, Sridhar [1 ]
Sun, Jun [2 ]
Williams, Jason [1 ]
Bachmann, Florian [2 ]
Gueninchault, Nicolas [2 ]
Lauridsen, Erik [2 ]
Chawla, Nikhilesh [1 ]
机构
[1] Arizona State Univ, Ctr 4D Mat Sci Mat Sci & Engn, 501 E Tyler Mall,ECG 303, Tempe, AZ 85287 USA
[2] Xnovo Technol ApS, Theilgaards 9 1th, DK-4600 Koge, Denmark
关键词
FATIGUE-CRACK GROWTH; X-RAY MICROTOMOGRAPHY; LOCALIZED CORROSION; BOUNDARY CHARACTER; 3D; MICROSTRUCTURE; PARTICLES; ALLOYS; LAPLACIAN; BEAM;
D O I
10.1007/s11837-019-03538-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Laboratory diffraction contrast tomography (LabDCT) is a laboratory-scale x-ray microtomography technique that can be used to non-destructively map grains and grain boundaries in 3D. The fidelity of grain mapping significantly depends on the quality of grain reflections obtained from the illuminated volume of the specimen. In this article, we report the application of a novel forward modeling approach to improve the reliability of grain mapping. Through this approach, a comparison between the obtained grain reflections and simulated grain reflections can be used to perform a self-fitting operation. This can be used to optimize instrumental parameters and iteratively improve the quality of reconstruction. To demonstrate the effectiveness of the forward modeling approach, LabDCT was used to map the grains in a polycrystalline specimen of the magnesium alloy AZ91E and iteratively improve reconstruction quality significantly.
引用
收藏
页码:2695 / 2704
页数:10
相关论文
共 49 条
[1]   Grain boundary structure, chemistry, and failure [J].
Briant, CL .
MATERIALS SCIENCE AND TECHNOLOGY, 2001, 17 (11) :1317-1323
[2]   Metal precipitation at grain boundaries in silicon: Dependence on grain boundary character and dislocation decoration [J].
Buonassisi, T. ;
Istratov, A. A. ;
Pickett, M. D. ;
Marcus, M. A. ;
Ciszek, T. F. ;
Weber, E. R. .
APPLIED PHYSICS LETTERS, 2006, 89 (04)
[3]   Large volume serial section tomography by Xe Plasma FIB dual beam microscopy [J].
Burnett, T. L. ;
Kelley, R. ;
Winiarski, B. ;
Contreras, L. ;
Daly, M. ;
Gholinia, A. ;
Burke, M. G. ;
Withers, P. J. .
ULTRAMICROSCOPY, 2016, 161 :119-129
[4]  
Chan LH, 2009, CERAM TRANS, V201, P261
[5]   APPLICATION OF GRAIN-BOUNDARY ENGINEERING CONCEPTS TO ALLEVIATE INTERGRANULAR CRACKING IN ALLOYS-600 AND ALLOYS-690 [J].
CHEUNG, C ;
ERB, U ;
PALUMBO, G .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1994, 185 (1-2) :39-43
[6]   In situ monitoring of corrosion processes within the bulk of AlMgSi alloys using X-ray microtomography [J].
Eckermann, Fabian ;
Suter, Thomas ;
Uggowitzer, Peter J. ;
Afseth, Andreas ;
Davenport, Alison J. ;
Connolly, Brian J. ;
Larsen, Magnus Hurlen ;
De Carlo, Francesco ;
Schmutz, Patrik .
CORROSION SCIENCE, 2008, 50 (12) :3455-3466
[7]  
Forsyth BCP, 1946, NAT PUBL GR, V158, P875, DOI [10.1038/158875a0, DOI 10.1038/158875A0]
[8]  
Gleiter H., 1981, Proc. 2nd Riso. Int. Symposium on Metall. and Mater. Sci, P15
[9]   Diffraction characterization of microstructure scale fatigue crack growth in a modern Al-Zn-Mg-Cu alloy [J].
Gupta, Vipul K. ;
Gangloff, Richard P. ;
Agnew, Sean R. .
INTERNATIONAL JOURNAL OF FATIGUE, 2012, 42 :131-146
[10]   Fatigue crack surface crystallography near crack initiating particle clusters in precipitation hardened legacy and modern Al-Zn-Mg-Cu alloys [J].
Gupta, Vipul K. ;
Agnew, Sean R. .
INTERNATIONAL JOURNAL OF FATIGUE, 2011, 33 (09) :1159-1174