Covalent bonding of phosphonates of L-proline and L-cysteine to γ-zirconium phosphate

被引：13

作者：

Huang, KL ^{[1
]}

Yu, JH ^{[1
]}

Wang, GM ^{[1
]}

Li, Y ^{[1
]}

Xu, RR ^{[1
]}

机构：

[1] Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China

来源：

EUROPEAN JOURNAL OF INORGANIC CHEMISTRY | 2004年 / 14期

关键词：

amino acids; chirality; phosphates; phosphonates; zirconium;

D O I：

10.1002/ejic.200300906

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

This paper describes the synthesis and characterization of gamma-zirconium phosphate-phosphonates based on chiral N-phosphonomethyl-L-proline [(-)-HO3PCH2NHC4H7CO2H; H3PMP] from L-proline, and N-phosphonomethyl-1,3-thiazolidine-4-carboxylic acid [(-)-HO3PCH2NHCH2SC2H3CO2H; H(3)PMTA] from L-cysteine. Two compounds formulated as [Zr(PO4)(H2PO4)(0.53)(H2PMP)(0.47).2.0H(2)O] [gamma-ZrPMP (1)] and [Zr(PO4)(H2PO4)(0.50)(H2PMT)(0.50).1.6H(2)O] [gamma-ZrPMT (2)] were obtained by topotactic reaction of H3PMP and H(3)PMTA, respectively, with gamma-ZrP in the presence of water/acetone. They possess intercalation capabilities and optical activities. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004).

引用

页码：2956 / 2960

页数：5

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