Synthesis, spectroscopic characterization, and X-ray crystal structure of tris(trimethylsilyl)cyanurate

被引：2

作者：

El-Gamel, Nadia E. A. ^{[1
]}

Brand, Joerg ^{[2
]}

Kroke, Edwin ^{[3
]}

机构：

[1] Cairo Univ, Fac Sci, Dept Chem, Giza 12613, Egypt

[2] Univ Konstanz, Dept Chem, D-78457 Constance, Germany

[3] Tech Univ Bergakad Freiberg, Inst Anorgan Chem, D-09596 Freiberg, Germany

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2009年 / 62卷 / 08期

关键词：

S-triazine; Tri-s-triazine; FTIR and Raman spectra; NMR; Thermal behavior; X-ray crystal structure; TRI-S-TRIAZINE; CYANURIC ACID; DERIVATIVES; INTERMEDIATE; CHEMISTRY; POLYMERS;

D O I：

10.1080/00958970802499372

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Tris(trimethylsilyl)cyanurate, C12H27N3O3Si3 (1), has been synthesized and characterized by elemental analysis, IR, Raman, 13C and 29Si NMR, and thermogravimetric methods. The molecular and crystal structure has been determined by single crystal X-ray diffraction. This compound crystallized in space group P63/m (176), Z = 2 with a = 11.017(2), b = 11.017(2), c = 9.676(3) ; = 90, = 90, = 120. The geometry of the molecule is compared with tris(trimethylsilyl)cyamelurate.

引用

页码：1278 / 1284

页数：7

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