Morphology and characterization studies of Y doped Bi-2212 single crystals

被引:3
作者
Prabhakaran, D
Thamizhavel, A
Subramanian, C
机构
[1] Crystal Growth Centre, Anna University, Madras
来源
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS | 1997年 / 288卷 / 3-4期
关键词
D O I
10.1016/S0921-4534(97)01591-8
中图分类号
O59 [应用物理学];
学科分类号
摘要
Superconducting Bi-2212 single crystals of nominal composition Bi2.2Sr1.9CaCu2O8, B2.1Y0.1Sr1.9CaCu2O8 and Bi2.2Sr1.9Ca0.9Y0.1Cu2O8 have been grown by flux method using a conical shaped Al2O3 crucible. Effect of Y doping on the crystal morphology has been studied. From the X-ray diffraction studies, the cell parameters were calculated. AC susceptibility showed that Y doping gives rise to highest T-c,T-onset at 92 K and the effect of annealing was also studied. The crystal composition at different places of the crucible and the Al incorporation were studied. The Sr/Ca ratio has been correlated with Y substitution. Chemical etching was also carried out on the grown crystals in order to reveal the nature of twinning and dislocations. (C) 1997 Elsevier Science B.V.
引用
收藏
页码:249 / 254
页数:6
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