Fe-based soft magnetic composites coated with NiZn ferrite prepared by a co-precipitation method

被引:73
作者
Peng, Yuandong [1 ]
Yi, Yi [1 ]
Li, Liya [1 ]
Ai, Hengyu [1 ]
Wang, Xiaoxu [1 ]
Chen, Lulu [2 ]
机构
[1] Cent S Univ, State Key Lab Powder Met, Changsha 410083, Hunan, Peoples R China
[2] Jiangsu Eagle Globe Grp Co Ltd, Nantong 226600, Peoples R China
基金
中国国家自然科学基金;
关键词
Soft magnetic composite; NiZn ferrite; Co-precipitation method; Insulation coating; Magnetic properties; SOL-GEL METHOD; ZN FERRITE; LOSS SEPARATION; HEAT-TREATMENT; IRON; PERMEABILITY; NANOPARTICLES; PARTICLES; SPINEL;
D O I
10.1016/j.jmmm.2016.12.024
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Fe powder was coated with NiZn ferrite by a co-precipitation method using chlorate as the raw material. Soft magnetic composites were manufactured via compaction and heat treatment of the coated powder. The coated powder and heat treated powder were analysed using scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD) and Raman spectroscopy. Their magnetic properties were determined using a Quantum Design-Vibrating Sample Magnetometer (QD-VSM). The composites were analysed with SEM and EDS. The permeability and magnetic loss of the composites were measured with a B-H curve analyzer. The results show that, using the co-precipitation method, the raw precipitate was successfully prepared and coated the pure Fe powder and turned into spinel NiZn ferrite treated at 600 degrees C for 1 h. After heat treatment at 500. under air, the insulation coating layer of soft magnetic composite (SMC) was not destroyed and containing Fe, Ni, Zn and oxygen. The permeabilities of the SMC are stable at edge of the 2-200 kHz frequency range and the total loss was lower.
引用
收藏
页码:148 / 153
页数:6
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