Highly efficient and practical resolution of 1,1′-spirobiindane-7,7′-diol by inclusion crystallization with N-benzylcinchonidinium chloride

被引：86
作者：
Zhang, JH
Liao, J
Cui, X
Yu, KB
Zhu, J
Deng, JG [1 ]
Zhu, SF
Wang, LX
Zhou, QL
Chung, LW
Ye, T
机构：
[1] Hong Kong Polytech Univ, Open Lab Chirotechnol, Kowloon, Hong Kong, Peoples R China
[2] Hong Kong Polytech Univ, Dept Appl Biol & Chem Technol, Kowloon, Hong Kong, Peoples R China
[3] Univ Hong Kong, Dept Chem, Hong Kong, Hong Kong, Peoples R China
[4] Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610041, Peoples R China
[5] Nankai Univ, State Key Lab, Tianjin 300071, Peoples R China
[6] Nankai Univ, Inst Elementoorgan Chem, Tianjin 300071, Peoples R China
来源：
TETRAHEDRON-ASYMMETRY | 2002年 / 13卷 / 13期
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1016/S0957-4166(02)00360-9
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The chiral spirobiindane ligand, 1,1'-spirobiindane-7,7'-diol has been resolved efficiently by inclusion complexation with commercially available N-benzylcinchonidinium chloride. The resolved complex was Studied by X-ray crystallography in order to characterize the intermolecular interactions and recognition nature. (C) 2002 Elsevier Science Ltd. All rights reserved.
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页码：1363 / 1366
页数：4
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