Preparation of high strength porous mullite ceramics via combined foam-gelcasting and microwave heating

被引:81
作者
Han, Lei [1 ]
Deng, Xiangong [1 ,2 ]
Li, Faliang [1 ]
Huang, Liang [1 ]
Pei, Yuantao [1 ]
Dong, Longhao [1 ]
Li, Saisai [1 ]
Jia, Quanli [3 ]
Zhang, Haijun [1 ]
Zhang, Shaowei [4 ]
机构
[1] Wuhan Univ Sci & Technol, State Key Lab Refractories & Met, Wuhan 430081, Hubei, Peoples R China
[2] Anhui Univ Technol, Sch Mat Sci & Engn, Maanshan 243002, Peoples R China
[3] Zhengzhou Univ, High Temp Ceram Inst, Zhengzhou 450052, Henan, Peoples R China
[4] Univ Exeter, Coll Engn Math & Phys Sci, Exeter EX4 4QF, Devon, England
基金
中国国家自然科学基金;
关键词
Mullite; Porous ceramics; High strength; Foam-gelcasting; Microwave heating method; LOW THERMAL-CONDUCTIVITY; CARBOTHERMAL REDUCTION; SINTERING TEMPERATURE; MOLTEN-SALT; SOL-GEL; POWDERS; ALUMINA; DENSIFICATION; PERFORMANCE; MORPHOLOGY;
D O I
10.1016/j.ceramint.2018.05.101
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Porous mullite ceramics with improved mechanical strength were fabricated by using a combined foam-gelcasting and microwave firing method at 1373-1523 K for 30 min. The porous mullite prepared at 1373 K contained 76.6% porosity, and exhibited flexural and compressive strength values as high as respectively 3.8 and 15.2 MPa. Moreover, its thermal conductivity still remained as low as 0.269 W/(m K). These values were comparable or even superior to those of porous mullite ceramics prepared previously via conventional heating at much higher temperatures (1573-1873 K), indicating that it is more beneficial to use microwave heating instead of conventional heating to make high quality porous mullite ceramics at a much lowered temperature.
引用
收藏
页码:14728 / 14733
页数:6
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