The Effect of Time between Handling and Photoactivation on Self-Adhesive Resin Cement Properties

被引:4
作者
Quirino da Silva Fonseca, Andrea Soares [1 ,2 ,4 ]
Mizrahi, Jamil [2 ]
Menezes, Livia Rodrigues [3 ]
Valente, Lisia Lorea [4 ]
de Moraes, Rafael Ratto [4 ]
Schneider, Luis Felipe [2 ,5 ]
机构
[1] Univ Fed Rio de Janeiro, Sch Dent, Dept Pediat Dent & Orthodont, Rio De Janeiro, Brazil
[2] Univ Veiga de Almeida, Sch Dent, Oral Rehabil Area, BR-20271020 Rio De Janeiro, RJ, Brazil
[3] Univ Fed Rio de Janeiro, Inst Macromol, Rio De Janeiro, Brazil
[4] Univ Fed Pelotas, Sch Dent, Grad Program Dent, Pelotas, Brazil
[5] Univ Fed Fluminense, Sch Dent, Dept Restorat Dent, Niteroi, RJ, Brazil
来源
JOURNAL OF PROSTHODONTICS-IMPLANT ESTHETIC AND RECONSTRUCTIVE DENTISTRY | 2014年 / 23卷 / 04期
关键词
Self-adhesive resin cement; water sorption; solubility; POLYMERIZATION CHARACTERISTICS; LIGHT-ACTIVATION; CURING MODE; COMPOSITE; SYSTEMS; DIMETHACRYLATE; THICKNESS; MONOMERS; SORPTION; WATER;
D O I
10.1111/jopr.12108
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
Purpose To evaluate the degree of conversion, absorption, and solubility in water of self-adhesive resin cements subjected to different time intervals between material preparation and the photoactivation procedure. Materials and Methods Two dual self-adhesive resin cements were tested: RelyX Unicem and SmartCem2. The degree of conversion as a function of time was evaluated by Fourier-transformed infrared spectroscopy using the attenuated total reflectance technique. Three time intervals between handling and photoactivation were applied: Group 1 = immediately; Group 2 = a 1-minute interval; Group 3 = a 4-minute interval. All specimens were irradiated with a light-emitting diode source for 40 seconds. Thirty discs of each cement (1 mm thick x 6 mm diameter, n = 10) were prepared for the absorption and solubility tests. These specimens were stored in distilled water at 37 degrees C for 90 days. The results were subjected to ANOVA with two factors (material and activation time intervals) and Tukey's test (95% significance). Results The 4-minute interval significantly reduced the degree of conversion of SmartCem2 (30.6% +/- 8.3%). No other significant changes were observed for the degree of conversion; however, the time intervals before photoactivation interfered significantly in the water absorption of the RelyX Unicem specimens but not the SmartCem2 specimens. The time intervals did not affect the solubility of either cement. In all cases, SmartCem2 had higher solubility than RelyX Unicem. Conclusion The time interval between handling and photoactivation significantly influenced the degree of conversion and water sorption of the resin-based cements. In general, one can say that the self-adhesive resin cements should be photoactivated as soon as possible after the material handling process.
引用
收藏
页码:302 / 307
页数:6
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