Influence of process variables on internal particle structure in spray fluidized bed agglomeration

被引:39
作者
Dadkhah, M. [1 ]
Tsotsas, E. [1 ]
机构
[1] Univ Magdeburg, D-39106 Magdeburg, Germany
关键词
Fluidized bed agglomeration; X-ray computed tomography; Morphological descriptors; Drying rate; Binder mass fraction; WET GRANULATION; GROWTH; KINETICS; BINDER; MODEL; SIZE;
D O I
10.1016/j.powtec.2014.03.005
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
In order to enhance and control properties of aggregates and be able to predict the structure of final products, it is essential to establish a link between the product properties and the operating conditions. Experimental investigations have been conducted on agglomerates produced in spray fluidized beds using different primary materials (non-porous glass, porous ceramic) and HPMC (hydroxyl-propyl-methyl-cellulose) as the binder, under varying operating conditions, inlet gas temperature and binder concentration. X-ray mu-computed tomography, mu-CT, was utilized to evaluate the three dimensional micro-structure of the agglomerates and spatial distribution of each constituent primary particle in the aggregate. Values and the behavior of evaluated morphological descriptors are presented and discussed for different agglomerates. (C) 2014 Elsevier B.V. All rights reserved,
引用
收藏
页码:165 / 173
页数:9
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