Liquid chromatographic method for the analysis of two plant based insecticide synergists dillapiole and dihydrodillapiole

被引：20

作者：

Walia, S ^{[1
]}

Saha, S ^{[1
]}

Parmar, BS ^{[1
]}

机构：

[1] Indian Agr Res Inst, Div Agr Chem, New Delhi 110012, India

来源：

JOURNAL OF CHROMATOGRAPHY A | 2004年 / 1047卷 / 02期

关键词：

Anethum sowa; dillapiole; dihydrodillapiole; pesticides;

D O I：

10.1016/j.chroma.2004.07.009

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A reversed-phase LC method for the determination of two plant based insecticide synergists dillapiole (5-allyl 6,7-dimethoxy 1,3-benzodioxole) and dihydrodillapiole (5-n-propyl 6,7-dimethoxy-1,3-benzodioxole) is reported. The resolution of dillapiole and dihydrodillapiole has been achieved on RP-18 column using methanol-water (90:10, v/v) as mobile phase and a photodiode array detector at 207 nm. The response was linear in the range of 25-250 mug. The developed isocratic RP-LC method was validated for specificity, linearity, precision, and accuracy. It has been applied for individual or simultaneous detection, monitoring and quantification of dillapiole and dihydrodillapiole from treated French bean Phaseolus sp. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：229 / 233

页数：5

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