Response Surface Methodology to Supercritical Carbon Dioxide Extraction of Essential Oil from Amormum krevanh Pierre

被引：4

作者：

Yothipitak, Wipawee ^{[1
]}

Goto, Motonobu ^{[2
]}

Tonanon, Nattanporn ^{[1
]}

Boonnoun, Panatpong ^{[1
]}

Shotipruk, Artiwan ^{[1
]}

机构：

[1] Chulalongkorn Univ, Dept Chem Engn, Fac Engn, Bangkok 10330, Thailand

[2] Kumamoto Univ, Dept Appl Chem & Biochem, Kumamoto, Japan

来源：

SEPARATION SCIENCE AND TECHNOLOGY | 2009年 / 44卷 / 16期

关键词：

Cardamom; 1; 8-cineole; extraction; optimization; orthogonal design; FLUID EXTRACTION; CO2; EXTRACT; CARDAMOM;

D O I：

10.1080/01496390903255788

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Response surface methodology was employed to investigate the effects of operating conditions and predict the optimal conditions for supercritical carbon dioxide extraction of essential oil from Amomum krevanh Pierre. The factors investigated were operating temperature (33-67 degrees C), the operating pressure (91-259bar), and the extraction time (20-70min). The main effect of the operating pressure and the interaction effect between the operating temperature and the extraction time were found to be significant factors. From the response surface model, an optimal condition for essential oil content within the range of experimental study was found to be at 33 degrees C, 175bar, and 70min, which gave the oil yield of 17.3mg/g dry wt. The essential oil yield obtained at all conditions were higher than that obtained by organic solvent extraction (9.74mg/g dry wt.) while the composition of the extract was similar, which were 1,8-cineole (70.87%), -pinene (8.89%), and limonene (4.81%).

引用

页码：3923 / 3936

页数：14

共 16 条

[1] Supercritical CO2 extractionof Salvia officinalis L. [J].

Aleksovski, S. A. ;

Sovova, H. .

JOURNAL OF SUPERCRITICAL FLUIDS, 2007, 40 (02) :239-245

[2] CRYOGENICALLY COOLED ADSORBENT TRAP FOR OFF-LINE SUPERCRITICAL FLUID EXTRACTION [J].

ASHRAFKHORASSANI, M ;

HOUCK, RK ;

LEVY, JM .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1992, 30 (09) :361-366

[3] Supercritical fluid extraction for liquid chromatographic determination of carotenoids in Spirulina Pacifica algae: a chemometric approach [J].

Careri, M ;

Furlattini, L ;

Mangia, A ;

Musci, M ;

Anklam, E ;

Theobald, A ;

von Holst, C .

JOURNAL OF CHROMATOGRAPHY A, 2001, 912 (01) :61-71

[4] Supercritical carbon dioxide extraction of Angelica archangelica L. root oil [J].

Doneanu, C ;

Anitescu, G .

JOURNAL OF SUPERCRITICAL FLUIDS, 1998, 12 (01) :59-67

[5] Chemical composition of the essential oil and super critical CO2 extracts of Zataria multiflora Boiss [J].

Ebrahimzadeh, H ;

Yamini, Y ;

Sefidkon, F ;

Chaloosi, D ;

Pourmortazavi, SM .

FOOD CHEMISTRY, 2003, 83 (03) :357-361

[6] Comparative analysis of the oil and supercritical CO2 extract of Artemisia sieberi [J].

Ghasemi, Ensieh ;

Yamini, Yadollah ;

Bahramifar, Nader ;

Sefidkon, Fatemmeh .

JOURNAL OF FOOD ENGINEERING, 2007, 79 (01) :306-311

[7] SUPERCRITICAL CARBON-DIOXIDE EXTRACTION OF CARDAMOM [J].

GOPALAKRISHNAN, N ;

NARAYANAN, CS .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1991, 39 (11) :1976-1978

[8] Comparison of essential oil composition of Carum copticum obtained by supercritical carbon dioxide extraction and hydrodistillation methods [J].

Khajeh, M ;

Yamini, Y ;

Sefidkon, F ;

Bahramifar, N .

FOOD CHEMISTRY, 2004, 86 (04) :587-591

[9] Correlation of binary diffusion coefficients of organic substances in supercritical carbon dioxide based on equations of state [J].

Kraska, T. ;

Quinones-Cisneros, S. E. ;

Deiters, U. K. .

JOURNAL OF SUPERCRITICAL FLUIDS, 2007, 42 (02) :212-218

[10] Solvent free microwave extraction of Elletaria cardamomum L.:: A multivariate study of a new technique for the extraction of essential oil [J].

Lucchesi, Marie E. ;

Smadja, Jacqueline ;

Bradshaw, Steven ;

Louw, Willem ;

Chemat, Farid .

JOURNAL OF FOOD ENGINEERING, 2007, 79 (03) :1079-1086

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