An instrument for in situ coherent x-ray studies of metal-organic vapor phase epitaxy of III-nitrides

被引:12
作者
Ju, Guangxu [1 ]
Highland, Matthew J. [1 ]
Yanguas-Gil, Angel [2 ]
Thompson, Carol [3 ]
Eastman, Jeffrey A. [1 ]
Zhou, Hua [4 ]
Brennan, Sean M. [5 ]
Stephenson, G. Brian [1 ]
Fuoss, Paul H. [1 ]
机构
[1] Argonne Natl Lab, Div Mat Sci, 9700 S Cass Ave, Argonne, IL 60439 USA
[2] Argonne Natl Lab, Div Energy Syst, 9700 S Cass Ave, Argonne, IL 60439 USA
[3] Northern Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
[4] Argonne Natl Lab, Xray Sci Div, 9700 S Cass Ave, Argonne, IL 60439 USA
[5] Fairview Associates, Jackson, WY 83002 USA
关键词
THERMAL-CONDUCTIVITY; GAN; SCATTERING; GROWTH; DIFFRACTION; NUCLEATION; DEPOSITION;
D O I
10.1063/1.4978656
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We describe an instrument that exploits the ongoing revolution in synchrotron sources, optics, and detectors to enable in situ studies of metal-organic vapor phase epitaxy (MOVPE) growth of III-nitride materials using coherent x-ray methods. The system includes high-resolution positioning of the sample and detector including full rotations, an x-ray transparent chamber wall for incident and diffracted beam access over a wide angular range, and minimal thermal sample motion, giving the sub-micron positional stability and reproducibility needed for coherent x-ray studies. The instrument enables surface x-ray photon correlation spectroscopy, microbeam diffraction, and coherent diffraction imaging of atomic-scale surface and film structure and dynamics during growth, to provide fundamental understanding of MOVPE processes. Published by AIP Publishing.
引用
收藏
页数:13
相关论文
共 37 条
  • [2] [Anonymous], GE ADV CER CORP MOM
  • [3] [Anonymous], COMMUNICATION
  • [4] [Anonymous], 1998, J. Phys. Chem. Ref. Data, Mono.
  • [5] EXPERIMENTAL CONSIDERATIONS FOR INSITU X-RAY-SCATTERING ANALYSIS OF OMVPE GROWTH
    BRENNAN, S
    FUOSS, PH
    KAHN, JL
    KISKER, DW
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1990, 291 (1-2) : 86 - 92
  • [6] Ferziger M., 1999, Computational Methods for Fluid Dynamics
  • [7] FUOSS PH, 1990, ANNU REV MATER SCI, V20, P365
  • [8] Ion-assisted nucleation and growth of GaN on sapphire(0001)
    Headrick, RL
    Kycia, S
    Woll, AR
    Brock, JD
    Murty, MVR
    [J]. PHYSICAL REVIEW B, 1998, 58 (08): : 4818 - 4824
  • [9] Thermal diffusivity and thermal conductivity of single-crystal MgO and Al2O3 and related compounds as a function of temperature
    Hofmeister, Anne M.
    [J]. PHYSICS AND CHEMISTRY OF MINERALS, 2014, 41 (05) : 361 - 371
  • [10] Quantitative Nanoscale Imaging of Lattice Distortions in Epitaxial Semiconductor Heterostructures Using Nanofocused X-ray Bragg Projection Ptychography
    Hruszkewycz, S. O.
    Holt, M. V.
    Murray, C. E.
    Bruley, J.
    Holt, J.
    Tripathi, A.
    Shpyrko, O. G.
    McNulty, I.
    Highland, M. J.
    Fuoss, P. H.
    [J]. NANO LETTERS, 2012, 12 (10) : 5148 - 5154