Five-year survey of ochratoxin A in processed sultanas from Turkey

被引:48
作者
Aksoy, U.
Eltem, R.
Meyvaci, K. B. [1 ]
Altindisli, A.
Karabat, S.
机构
[1] Fac Agr, Dept Hort, TR-35100 Izmir, Turkey
[2] Fac Engn, Dept Bioengn, TR-35100 Izmir, Turkey
[3] Ctr Res & Dev, TARIS Union Farmers Sales Cooperat, TR-35100 Izmir, Turkey
来源
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT | 2007年 / 24卷 / 03期
关键词
ochratoxin A; high-performance liquid chromatography (HPLC); dried vine fruits; processed sultana raisins; mycotoxin;
D O I
10.1080/02652030601039021
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The results of surveillance for ochratoxin A (OTA) in 1885 samples of sultanas taken during five crop years between 1999 and 2003 are reported. The analytical method was based on extraction with methanol+sodium bicarbonate and clean-up by immunoaffinity column chromatography followed by high-performance liquid chromatography with fluorescence detection. The limit of detection for OTA was 0.3 mg kg(-1). The results show that 9.3% of the samples contained no detectable levels of OTA, whereas 0.6% had concentrations exceeding 10 mu g kg(-1); the remaining 90.3% had levels within the range 0.3 - 10 mu gkg(-1). The overall mean OTA concentration in the total number of 1885 samples taken was 1.36 +/- 2.91 mu g kg(-1); the overall median was calculated as 0.90 mu g kg(-1).
引用
收藏
页码:292 / 296
页数:5
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