Synthesis and characterization of mesoporous Co-SiO2 spheres with high surface area

被引:0
|
作者
Zhang, P [1 ]
Liu, YL [1 ]
Bai, N [1 ]
Fu, YL [1 ]
Li, SG [1 ]
Meng, XJ [1 ]
Ding, H [1 ]
Pang, WQ [1 ]
机构
[1] Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
来源
CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE | 2002年 / 23卷 / 08期
关键词
mesoporous Co-SiO2 spheres; complex of metal ion-aminosilane; synthesis at room temperature;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In basic media, millimeter-sized mesoporous Co-SiO2 spheres were synthesized successfully through the introduction of Co(III)-APTMOS complex into the reaction mixture with cetyltrimethylammonium bromide(CTAB) as a structural template. The products are characterized by N-2 adsorption, HRTEM, SEM, and ICP techniques. The results show that the mesoporous Co-SiO2 spheres have a high surface area and disordered pores. Furthermore, the advantage of using Co(III)-APTMOS complex as the source of metal element Co is discussed.
引用
收藏
页码:1466 / 1469
页数:4
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