Synthesis and characterization of mesoporous Co-SiO2 spheres with high surface area
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作者:
Zhang, P
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机构:
Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Zhang, P
[1
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Liu, YL
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Liu, YL
[1
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Bai, N
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Bai, N
[1
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Fu, YL
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Fu, YL
[1
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Li, SG
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Li, SG
[1
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Meng, XJ
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Meng, XJ
[1
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Ding, H
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Ding, H
[1
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Pang, WQ
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Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R ChinaJilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
Pang, WQ
[1
]
机构:
[1] Jilin Univ, State Key Lab Inorgan Synth & Perparat Chem, Changchun 130023, Peoples R China
来源:
CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
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2002年
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23卷
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08期
关键词:
mesoporous Co-SiO2 spheres;
complex of metal ion-aminosilane;
synthesis at room temperature;
D O I:
暂无
中图分类号:
O6 [化学];
学科分类号:
0703 ;
摘要:
In basic media, millimeter-sized mesoporous Co-SiO2 spheres were synthesized successfully through the introduction of Co(III)-APTMOS complex into the reaction mixture with cetyltrimethylammonium bromide(CTAB) as a structural template. The products are characterized by N-2 adsorption, HRTEM, SEM, and ICP techniques. The results show that the mesoporous Co-SiO2 spheres have a high surface area and disordered pores. Furthermore, the advantage of using Co(III)-APTMOS complex as the source of metal element Co is discussed.