Production of graphene layer by liquid-phase exfoliation with low sonication power and sonication time from synthesized expanded graphite

被引:73
作者
Guler, Omer [1 ]
Guler, S. Hale [2 ]
Selen, Veyis [3 ]
Albayrak, M. Gokhan [1 ]
Evin, Ertan [1 ]
机构
[1] Firat Univ, Dept Met & Mat Engn, TR-23169 Elazig, Turkey
[2] Mersin Univ, Dept Met & Mat Engn, Mersin, Turkey
[3] Firat Univ, Dept Chem Engn, TR-23169 Elazig, Turkey
关键词
Graphene; liquid-phase exfoliation; expanded graphite; BIPOLAR PLATE; HIGH-QUALITY; FILMS; NANOSHEETS; ELECTRODE; SHEETS; YIELD;
D O I
10.1080/1536383X.2015.1114472
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Multi-layer graphene was produced through synthesized expanded graphite (EG) liquid exfoliation using organic solvent. Hexagonal graphite (HG) was used as a starting material. HG was mixed with an acidic mixture, dried, rand subjected to thermal treatment. After this process, EG was obtained. This obtained EG was sonicated for 1h via an ultrasonic homogenizer by blending an organic solvent. Samples were subjected to SEM, TEM, FTIR, and UV-Vis/NIR spectroscopy investigations. After the investigations, it was shown that nano-size graphene sheets were obtained.
引用
收藏
页码:123 / 127
页数:5
相关论文
共 29 条
[1]   Size-controlled synthesis of graphite nanoflakes and multi-layer graphene by liquid phase exfoliation of natural graphite [J].
Alaferdov, A. V. ;
Gholamipour-Shirazi, A. ;
Canesqui, M. A. ;
Danilov, Yu. A. ;
Moshkalev, S. A. .
CARBON, 2014, 69 :525-535
[2]  
Bae S, 2010, NAT NANOTECHNOL, V5, P574, DOI [10.1038/NNANO.2010.132, 10.1038/nnano.2010.132]
[3]   Electronic confinement and coherence in patterned epitaxial graphene [J].
Berger, Claire ;
Song, Zhimin ;
Li, Xuebin ;
Wu, Xiaosong ;
Brown, Nate ;
Naud, Cecile ;
Mayou, Didier ;
Li, Tianbo ;
Hass, Joanna ;
Marchenkov, Atexei N. ;
Conrad, Edward H. ;
First, Phillip N. ;
de Heer, Wait A. .
SCIENCE, 2006, 312 (5777) :1191-1196
[4]  
Carreira L., 2013, MAT SCI APPL, V4, P281, DOI DOI 10.4236/MSA.2013.45035
[5]   Graphite Oxide and Graphene Nanoribbons Reduction with Hydrogen Iodide [J].
Cataldo, Franco ;
Ursini, Ornella ;
Angelini, Giancarlo .
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES, 2011, 19 (05) :461-468
[6]   Characterization of Graphene Nanosheets as Electrode Material and Their Performances for Electric Double-Layer Capacitors [J].
Chen, Ming-Liang ;
Park, Chong-Yeon ;
Meng, Za-Da ;
Zhu, Lei ;
Choi, Jong-Geun ;
Ghosh, Trisha ;
Kim, Ick-Jun ;
Yang, Sunhye ;
Bae, Mi-Kyung ;
Zhang, Feng-Jun ;
Oh, Won-Chun .
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES, 2013, 21 (06) :525-536
[7]   Liquid-phase exfoliation, functionalization and applications of graphene [J].
Cui, Xu ;
Zhang, Chenzhen ;
Hao, Rui ;
Hou, Yanglong .
NANOSCALE, 2011, 3 (05) :2118-2126
[8]   Development and characterization of expanded graphite-based nanocomposite as bipolar plate for polymer electrolyte membrane fuel cells (PEMFCs) [J].
Dhakate, S. R. ;
Shanna, S. ;
Borah, A. ;
Mathur, R. B. ;
Dhami, T. L. .
ENERGY & FUELS, 2008, 22 (05) :3329-3334
[9]   An approach to produce single and double layer graphene from re-exfoliation of expanded graphite [J].
Dhakate, S. R. ;
Chauhan, N. ;
Sharma, S. ;
Tawale, J. ;
Singh, S. ;
Sahare, P. D. ;
Mathur, R. B. .
CARBON, 2011, 49 (06) :1946-1954
[10]   Expanded graphite-based electrically conductive composites as bipolar plate for PEM fuel cell [J].
Dhakate, S. R. ;
Sharma, S. ;
Borah, M. ;
Mathur, R. B. ;
Dhami, T. L. .
INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2008, 33 (23) :7146-7152