Synthesis and characterization of uniform fine particles of copper oxalate

被引:11
作者
ul Haq, Ikram [1 ]
Haider, Farzana [1 ]
机构
[1] Univ Peshawar, Natl Ctr Excellence Phys Chem, Peshawar 25120, NWFP, Pakistan
关键词
Copper oxalate; Isoelectric point (IEP); Fine particles; THERMAL-DECOMPOSITION; CUO;
D O I
10.1016/j.matlet.2009.08.008
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Copper oxalate particles were synthesized in various shapes and sizes by mixing appropriate volumes of known concentration of oxalic acid and copper nitrate at 25 and 85 degrees C. Temperature and reactants concentration had significant effect on the morphology of the precipitated particles and therefore extensive optimizations of the experimental parameters were carried out in order to obtain maximum uniformity in particles' morphological features. Selected batch of the copper oxalate particles was characterized by various physical methods. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:2355 / 2357
页数:3
相关论文
共 15 条
  • [1] Tin dioxide nanoparticles: Reverse micellar synthesis and gas sensing properties
    Ahmed, Jahangeer
    Vaidya, Sonalika
    Ahmad, Tokeer
    Devi, P. Sujatha
    Das, Dipankar
    Ganguli, Ashok K.
    [J]. MATERIALS RESEARCH BULLETIN, 2008, 43 (02) : 264 - 271
  • [2] Rapid nickel oxalate thermal decomposition for producing fine porous nickel metal powders Part 1: Synthesis
    Carney, C. S.
    Gump, C. J.
    Weimer, A. W.
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2006, 431 (1-2): : 1 - 12
  • [3] Magnesium silicates - adsorbents of organic compounds
    Ciesielczyk, Filip
    Krysztafkiewicz, Andrzej
    Jesionowski, Teofil
    [J]. APPLIED SURFACE SCIENCE, 2007, 253 (20) : 8435 - 8442
  • [4] State of the art of zirconia for dental applications
    Denry, Isabelle
    Kelly, J. Robert
    [J]. DENTAL MATERIALS, 2008, 24 (03) : 299 - 307
  • [5] HAQ I, 2003, COLLOID POLYM SCI, V281, P542
  • [6] Nanotechnology in action: Overbased nanodetergents as lubricant oil additives
    Hudson, L. K.
    Eastoe, J.
    Dowding, P. J.
    [J]. ADVANCES IN COLLOID AND INTERFACE SCIENCE, 2006, 123 (425-431) : 425 - 431
  • [7] The convenient preparation of porous CuO via copper oxalate precursor
    Jia, Zhigang
    Yue, Linhai
    Zheng, Yifan
    Xu, Zhude
    [J]. MATERIALS RESEARCH BULLETIN, 2008, 43 (8-9) : 2434 - 2440
  • [8] Calcination and morphological evolution of cubic copper oxalate particles
    Jongen, N
    Hofmann, H
    Bowen, P
    Lemaître, J
    [J]. JOURNAL OF MATERIALS SCIENCE LETTERS, 2000, 19 (12) : 1073 - 1075
  • [9] Biologically active core/shell nanoparticles self-assembled from cholesterol-terminated PEG-TAT for drug delivery across the blood-brain barrier
    Li, Lihong
    Guo, Kun
    Lu, Jia
    Venkatraman, Subbu S.
    Luo, Dan
    Ng, Kian Chye
    Ling, Eng-Ang
    Moochhala, Shabbir
    Yang, Yi-Yan
    [J]. BIOMATERIALS, 2008, 29 (10) : 1509 - 1517
  • [10] EXAFS DETERMINATION OF THE COPPER OXALATE STRUCTURE - RELATION BETWEEN STRUCTURE AND MAGNETIC-PROPERTIES
    MICHALOWICZ, A
    GIRERD, JJ
    GOULON, J
    [J]. INORGANIC CHEMISTRY, 1979, 18 (11) : 3004 - 3010