Chiral separation of racemic thiols based on diastereomer formation with a fluorescent chiral tagging reagent by reversed-phase liquid chromatography

被引：13

作者：

Jin, DR ^{[1
]}

Takehana, K ^{[1
]}

Toyooka, T ^{[1
]}

机构：

[1] UNIV SHIZUOKA, SCH PHARMACEUT SCI, DEPT ANALYT CHEM, YADA, SHIZUOKA 422, JAPAN

来源：

ANALYTICAL SCIENCES | 1997年 / 13卷 / 01期

关键词：

racemic thiol; precolumn derivatization; diastereomer formation; fluorescence detection; reversed-phase liquid chromatography;

D O I：

10.2116/analsci.13.113

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

[No abstract available]

引用

页码：113 / 115

页数：3

共 11 条

[1]

GPROG S, 1994, J CHROMATOGR B, V659, P51

[2] RESOLUTION OF THE ENANTIOMERS OF THIOL COMPOUNDS BY REVERSED-PHASE LIQUID-CHROMATOGRAPHY USING CHIRAL DERIVATIZATION WITH 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSYL ISOTHIOCYANATE [J].

ITO, S ;

OTA, A ;

YAMAMOTO, K ;

KAWASHIMA, Y .

JOURNAL OF CHROMATOGRAPHY, 1992, 626 (02) :187-196

[3]

KRSTULOVIC AM, 1989, CHIRAL SEPARATION HP

[4] OPTICAL RESOLUTION OF THIOL ENANTIOMERS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY USING PRECOLUMN FLUORESCENCE DERIVATIZATION WITH O-PHTHALALDEHYDE AND ALPHA-AMINO-ACIDS [J].

SANO, A ;

TAKITANI, S ;

NAKAMURA, H .

ANALYTICAL SCIENCES, 1995, 11 (02) :299-301

[5] CHIRAL SEPARATION BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1. REVIEW ON INDIRECT SEPARATION OF ENANTIOMERS AS DIASTEREOMERIC DERIVATIVES USING ULTRAVIOLET, FLUORESCENCE AND ELECTROCHEMICAL DETECTION [J].

SRINIVAS, NR ;

IGWEMEZIE, LN .

BIOMEDICAL CHROMATOGRAPHY, 1992, 6 (04) :163-167

[6] DEVELOPMENT OF OPTICALLY-ACTIVE FLUORESCENT EDMAN-TYPE REAGENTS [J].

TOYOOKA, T ;

LIU, YM .

ANALYST, 1995, 120 (02) :385-390

[7]

Toyooka T, 1996, BIOMED CHROMATOGR, V10, P265, DOI 10.1002/(SICI)1099-0801(199611)10:6<265::AID-BMC602>3.0.CO

[8]

2-A

[9] Sequential analysis of D/L-amino acid in peptide with a novel chiral Edman degradation method [J].

Toyooka, T ;

Suzuki, T ;

Watanabe, T ;

Liu, YM .

ANALYTICAL SCIENCES, 1996, 12 (05) :779-782

[10] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC RESOLUTION OF AMINO-ACID ENANTIOMERS DERIVATIZED WITH FLUORESCENT CHIRAL EDMAN REAGENTS [J].

TOYOOKA, T ;

LIU, YM .

JOURNAL OF CHROMATOGRAPHY A, 1995, 689 (01) :23-30

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