Preparation of barium strontium titanate Ba1-xSrxTiO3 (0 ≤ x ≤ 0.2) single-crystal nanorods by a novel combined method

被引：24

作者：

Jiang, Wanquan ^{[1
]}

Gong, Xiuqing

Chen, Zuyao

Hu, Yuan

Zhang, Xianzhou

Gong, Xinglong

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, State Key Lab Fire Sci, Hefei 230026, Anhui, Peoples R China

[3] Univ Sci & Technol China, Dept Mech Engn & Mech, Hefei 230026, Anhui, Peoples R China

来源：

ULTRASONICS SONOCHEMISTRY | 2007年 / 14卷 / 02期

关键词：

nanorods; barium strontium titanate; ultrasonic radiation; sol-gel method; sonogel;

D O I：

10.1016/j.ultsonch.2006.02.002

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

An ultrasonic irradiation method was applied to the sol/gel synthesis of the single-crystal cubic barium strontium titanate Ba1-xSrxTiO3 (0 <= x <= 0.2). The characteristics of the composites were examined by X-ray diffraction, thermogravimetric analysis, differential thermal analysis, transmission electron microscopy and high-resolution transmission microscopy. The diameters and lengths of typical resultant Ba0.8Sr0.2TiO3 are in the range of 70-100 nm and 650-1000 nm, respectively. In addition, the stoichiometric sonogel formation and its heat-treatment process, the relationship between x of Ba1-xSrxTiO (3) and the crystal structure, the relationship between synthesis condition of sonogel and morphology have been discussed. (C) 2006 Elsevier B.V. All rights reserved.

引用

页码：208 / 212

页数：5

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