Electron diffraction and imaging for atom probe tomography

被引:5
作者
Kirchhofer, Rita [1 ]
Diercks, David R. [1 ]
Gorman, Brian P. [1 ]
机构
[1] Colorado Sch Mines, Dept Met & Mat Engn, Golden, CO 80401 USA
基金
美国国家科学基金会;
关键词
FIELD EVAPORATION; MICROSCOPY;
D O I
10.1063/1.4999484
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Previous work has shown that pre- and post-experiment quantification of atom probe tomography (APT) specimen geometry using electron microscopy can constrain otherwise unknown parameters, leading to an improvement in data fidelity. To that end, an electron microscopy and diffraction system has been developed for in situ compatibility with modern APT hardware. The system is capable of secondary and backscattered scanning electron imaging, bright field and dark field scanning transmission electron imaging, and scanning transmission electron diffraction. Additionally, the system is also capable of in situ dynamic electron diffraction experiments using laser pulsed heating of the APT specimen. Published by AIP Publishing.
引用
收藏
页数:5
相关论文
共 25 条
[1]   A GENERAL PROTOCOL FOR THE RECONSTRUCTION OF 3D ATOM-PROBE DATA [J].
BAS, P ;
BOSTEL, A ;
DECONIHOUT, B ;
BLAVETTE, D .
APPLIED SURFACE SCIENCE, 1995, 87-8 (1-4) :298-304
[2]  
Diercks D. R., 2012, 53 INT FIELD EM S
[3]   Atom probe tomography evaporation behavior of C-axis GaN nanowires: Crystallographic, stoichiometric, and detection efficiency aspects [J].
Diercks, David R. ;
Gorman, Brian P. ;
Kirchhofer, Rita ;
Sanford, Norman ;
Bertness, Kris ;
Brubaker, Matt .
JOURNAL OF APPLIED PHYSICS, 2013, 114 (18)
[4]  
Gault B., 2012, Atom Probe Microscopy, V160
[5]   Advances in the calibration of atom probe tomographic reconstruction [J].
Gault, Baptiste ;
Moody, Michael P. ;
de Geuser, Frederic ;
Tsafnat, Guy ;
La Fontaine, Alexandre ;
Stephenson, Leigh T. ;
Haley, Daniel ;
Ringer, Simon P. .
JOURNAL OF APPLIED PHYSICS, 2009, 105 (03)
[6]   Cross-correlative TEM and atom probe analysis of partial crystallisation in NiNbSn metallic glasses [J].
Gorman, B. P. ;
Puthucode, A. ;
Diercks, D. R. ;
Kaufman, M. J. .
MATERIALS SCIENCE AND TECHNOLOGY, 2008, 24 (06) :682-688
[7]  
Gorman B.P., 2008, MICROS TODAY, V16, P42, DOI DOI 10.1017/S1551929500059782
[8]   Level Set Methods for Modelling Field Evaporation in Atom Probe [J].
Haley, Daniel ;
Moody, Michael P. ;
Smith, George D. W. .
MICROSCOPY AND MICROANALYSIS, 2013, 19 (06) :1709-1717
[9]   Ptychographic electron microscopy using high-angle dark-field scattering for sub-nanometre resolution imaging [J].
Humphry, M. J. ;
Kraus, B. ;
Hurst, A. C. ;
Maiden, A. M. ;
Rodenburg, J. M. .
NATURE COMMUNICATIONS, 2012, 3
[10]   The origin of electrical property deterioration with increasing Mg concentration in ZnMgO:Ga [J].
Ke, Yi ;
Berry, Joseph ;
Parilla, Philip ;
Zakutayev, Andriy ;
O'Hayre, Ryan ;
Ginley, David .
THIN SOLID FILMS, 2012, 520 (09) :3697-3702