Preparation of ZrO2-CeO2 and HfO2-CeO2 nanopowders

被引:5
作者
Glushkova, V. B. [1 ]
Panova, T. I. [1 ]
机构
[1] Russian Acad Sci, IV Grebenshchikov Silicate Chem Inst, St Petersburg 199155, Russia
关键词
Zirconia; Solid Solution; Crystallite Size; Hafnium; Mechanochemical Synthesis;
D O I
10.1134/S0020168506100050
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We prepared weakly agglomerated powders of ZrO2-CeO2 and HfO2-CeO2 solid solutions 5-8 nm in particle size, consisting of monoclinic and tetragonal phases. After heat treatment at 12000 degrees C, the crystallite size was 30 and 14 nm, respectively. We also examined the effect of precipitate freeze drying on the crystallization of hafnia-based solid solutions containing up to 20 mol % CeO2.
引用
收藏
页码:1076 / 1082
页数:7
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