Structural and spectral studies of 2-(3,4,5-trimethoxyphenyl)-benzothiazole

被引：4
|
作者：
Ide, S [1 ]
Oztas, SG [1 ]
Ancin, N [1 ]
Tuzun, M [1 ]
机构：
[1] ANKARA UNIV,DEPT CHEM,FAC SCI,ANKARA,TURKEY
来源：
CRYSTAL RESEARCH AND TECHNOLOGY | 1996年 / 31卷 / 04期
关键词：
D O I：
10.1002/crat.2170310405
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
2-(3,4,5-trimethoxyphenyl)-benzothiazole C16H15NO3S was obtained by condensation of 2-aminobenzenethiol with 3,4, 5-trimethoxybenzoldehyde. The structure of the title compound was indicated by IR, H-1-NMR, UV spectra and confirmed by an X-ray analysis. In the molecule the trimethoxyphenyl and benzothiazole groups are connected by a C-C bond of 1.478(6) Angstrom. The trimethoxyphenyl except a methoxy group and the benzothiazole group are nearly planar. The dihedral angle between these planes is 8.5(9)degrees.
引用
收藏
页码：429 / 433
页数：5
相关论文
共 50 条
  • [21] (Z)-3-(1H-Indol-3-yl)-2-(3,4,5-trimethoxyphenyl)acrylonitrile
    Penthala, Narsimha Reddy
    Parkin, Sean
    Crooks, Peter A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O729 - U2223
  • [22] (E)-4-[2-(3,4,5-Trimethoxyphenyl)ethenyl]nitrobenzene and its 'bridge-flipped' analogues
    Collas, Alain
    Blockhuys, Frank
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2011, 67 : O364 - O369
  • [23] Study of electroorganic synthesis of 1,4-bis[2-(3,4,5-trimethoxyphenyl)vinyl]benzene
    Qiu, XY
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2000, 20 (03) : 348 - 351
  • [24] Two pairs of stereoisomers of dimethyl 2-(3,4,5-trimethoxyphenyl)tetrahydrofuran-3,4-dicarboxylate
    Yang, QC
    Song, YQ
    Tang, YQ
    Pei, WW
    Li, SH
    Ye, XL
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 1133 - 1136
  • [25] Two pairs of stereoisomers of dimethyl 2-(3,4,5-trimethoxyphenyl)tetrahydrofuran-3,4-dicarboxylate
    Peking Univ, Beijing, China
    Acta Crystallogr Sect C Cryst Struct Commun, pt 8 (1133-1136):
  • [26] Studies on the reaction conditions and mechanism of electroorganic synthesis of 1,4-Bis[2-(3,4,5-trimethoxyphenyl)vinyl]benzene
    Qiu, XY
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2003, 23 (03) : 258 - 264
  • [27] Natural antitubulin agents: Importance of 3,4,5-trimethoxyphenyl fragment
    Negi, Arvind S.
    Gautam, Yashveer
    Alam, Sarfaraz
    Chanda, Debabrata
    Luqman, Suaib
    Sarkar, Jayanta
    Khan, Feroz
    Konwar, Rituraj
    BIOORGANIC & MEDICINAL CHEMISTRY, 2015, 23 (03) : 373 - 389
  • [28] A SYNTHESIS OF BETA-(3,4,5-TRIMETHOXYPHENYL)-PROPIONIC ACID
    GUTSCHE, CD
    HOYER, FA
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1950, 72 (09) : 4285 - 4286
  • [29] Ethyl 3-oxo-3-(3,4,5-trimethoxyphenyl)-propanoate
    Meng, XG
    Wu, AX
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3611 - O3612
  • [30] Ethyl N,N′-bis(3,4,5-trimethoxyphenyl)-phosphorodiamidate
    Li, Chenguang
    Robinson, Paul D.
    Dyer, Daniel J.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4233 - O4235
12345