Hard template route for synthesis of mesoporous spinel type oxides with ordered structure

被引：0

作者：

Shen, Weihua ^{[1
]}

机构：

[1] E China Univ Sci & Technol, Sch Chem Engn, Shanghai 200237, Peoples R China

来源：

ADVANCED RESEARCH ON MATERIAL SCIENCE, ENVIROMENT SCIENCE AND COMPUTER SCIENCE III | 2014年 / 886卷

关键词：

Hard template; Mesoporous spinel; Metal oxide; Mesoporous silica; SILICA;

D O I：

10.4028/www.scientific.net/AMR.886.200

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

The binary mesoporous spinel oxides with high surface area have been synthesized by. using KIT-6 and SBA-15 as hard templates and hydrated nitrated salts as precursors. Low temperature such as 500 degrees C is suitable for preparation of NiCo2O4 with spinel phase. High temperature such as 800 degrees C is necessary for preparation of NiMn2O4, MnCo2O4, and (Co0.5Mn0.5)(3)O-4 with pure spine! phase. The prepared mesoporous spinel shows high surface area as 43-105 m(2)/g with pore volume as 0.095-0.233 cm(3)/g. It is preferred to form mesoporous NiCo2O4 with spherical particles.

引用

页码：200 / 203

页数：4

共 50 条

[31] Template Synthesis of Three-Dimensional Cubic Ordered Mesoporous Carbon With Tunable Pore Sizes [J].

Dai, Weijie ;

Zheng, Mingbo ;

Zhao, Yu ;

Liao, Shutian ;

Ji, Guangbin ;

Cao, Jieming .

NANOSCALE RESEARCH LETTERS, 2010, 5 (01) :103-107

[32] Template Synthesis of Three-Dimensional Cubic Ordered Mesoporous Carbon With Tunable Pore Sizes [J].

Weijie Dai ;

Mingbo Zheng ;

Yu Zhao ;

Shutian Liao ;

Guangbin Ji ;

Jieming Cao .

Nanoscale Research Letters, 5

[33] Synthesis of ordered mesoporous alumina with large pore sizes and hierarchical structure [J].

Wu, Qingling ;

Zhang, Fan ;

Yang, Jianping ;

Li, Qiang ;

Tu, Bo ;

Zhao, Dongyuan .

MICROPOROUS AND MESOPOROUS MATERIALS, 2011, 143 (2-3) :406-412

[34] Hard template synthesis of crystalline mesoporous anatase TiO2 for photocatalytic hydrogen evolution [J].

Zhang, Zhenyu ;

Zuo, Fan ;

Feng, Pingyun .

JOURNAL OF MATERIALS CHEMISTRY, 2010, 20 (11) :2206-2212

[35] Hard-template Synthesis of Hollow Mesoporous Silica Nanoplates Using Layered Double Hydroxide [J].

Shi, Yue ;

Wang, Junzheng ;

Yamamoto, Eisuke ;

Osada, Minoru .

CHEMISTRY LETTERS, 2020, 49 (09) :1078-1080

[36] Synthesis of ordered mesoporous NiCo2O4 via hard template and its application as bifunctional electrocatalyst for Li-O2 batteries [J].

Li, Yuan ;

Zou, Liangliang ;

Li, Jun ;

Guo, Kun ;

Dong, Xiaowen ;

Li, Xiaowei ;

Xue, Xinzhong ;

Zhang, Haifeng ;

Yang, Hui .

ELECTROCHIMICA ACTA, 2014, 129 :14-20

[37] Synthesis of ordered mesoporous iron manganese bimetal oxides for arsenic removal from aqueous solutions [J].

Wen, Zhipan ;

Zhang, Yalei ;

Dai, Chaomeng ;

Chen, Bo ;

Guo, Sujin ;

Yu, Hong ;

Wu, Deli .

MICROPOROUS AND MESOPOROUS MATERIALS, 2014, 200 :235-244

[38] A Rational Repeating Template Method for Synthesis of 2D Hexagonally Ordered Mesoporous Precious Metals [J].

Takai, Azusa ;

Doi, Yoji ;

Yamauchi, Yusuke ;

Kuroda, Kazuyuki .

CHEMISTRY-AN ASIAN JOURNAL, 2011, 6 (03) :881-887

[39] Nanocasting Synthesis of Iron-Doped Mesoporous Al-Ti Mixed Oxides Using Ordered Mesoporous Carbon Templates [J].

Fulvio, Pasquale F. ;

Vinu, Ajayan ;

Jaroniec, Mietek .

JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 113 (31) :13565-13573

[40] Cage-like ordered mesoporous organosilicas with isocyanurate bridging groups: Synthesis, template removal and structural properties [J].

Grudzien, Rafal M. ;

Blitz, Jonathan P. ;

Pikus, Stanislaw ;

Jaroniec, Mietek .

MICROPOROUS AND MESOPOROUS MATERIALS, 2009, 118 (1-3) :68-77

← 1 2 3 4 5 →