X-ray diffraction analysis of aluminum hexamolybdenocobaltate(III) and hexamolybdenocromate(III)

被引：1
|
作者：
Kaziev, GZ
Quinones, SO
Bel'skii, VK
Zavodnik, VI
Osminkina, IV
De Ita, A
机构：
[1] Moscow State Pedag Univ, Moscow 119882, Russia
[2] LY Karpov Phys Chem Res Inst, Moscow 117333, Russia
来源：
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2002年 / 28卷 / 06期
关键词：
Aluminum; Physical Chemistry; Diffraction Analysis; Cell Parameter; Unit Cell Parameter;
D O I：
10.1023/A:1016020526090
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Isostructural crystals of aluminum hexamolybdenocobaltate(III) and hexamolybdenocromate(III) Al[MMo6O18(OH)(6)] (.) 16H(2)O (M = Co(III) and Cr(III)) were studied using X-ray diffraction analysis. These compounds crystallize in the triclinic system: space group P (1) over bar, Z = 1, p(calcd) = 2.665 and 2.611 g/cm(3), respectively. The unit cell parameters were determined: for aluminum hexamolybdenocobaltate(III), a = 6.796(1) Angstrom, b = 11.248(2) Angstrom, c = 11.568(2) Angstrom; alpha = 101.36(2)degrees, beta = 96.95(2)degrees, gamma = 102.23(2)degrees; for aluminum hexamolybdenocromate(III), a = 6.838(7) Angstrom, b = 11.312(2) Angstrom, c = 11.605(2) Angstrom; alpha = 101.29(3)degrees, beta = 97.13(3)degrees, gamma = 102.15(3)degrees.
引用
收藏
页码：384 / 388
页数：5
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