Electrochemical Rutin Sensor Based on Graphene Oxide and Functionalized Multiwall Carbon Nanotubes@nafion0.1% Hybrid Nanocomposite modified glassy carbon electrode

被引:3
|
作者
Kumar, Praveen G. [1 ]
Nehru, Raja [1 ]
Chen, Shen-Ming [1 ]
Almunqedhi, Bandar Mohsen [2 ]
Chen, Tse-Wei [1 ,3 ]
Wang, Jun-Yu [1 ]
Yu, Ming-Chin [4 ]
Darwish, Noura M. [5 ]
机构
[1] Natl Taipei Univ Technol, Dept Chem Engn & Biotechnol, Taipei 10608, Taiwan
[2] King Saud Univ, Dept Bot & Microbiol, Coll Sci, POB 2455, Riyadh 11451, Saudi Arabia
[3] Natl Taipei Univ Technol, Res & Dev Ctr Smart Text Technol, Taipei 106, Taiwan
[4] Chang Gung Mem Hosp, Dept Surg, Taoyuan 333, Taiwan
[5] Ain Shams Univ, Dept Biochem, Cairo 12311, Egypt
来源
关键词
Flavonoid; Antioxidant; GO; f-MWCNTs; Hummer's method; and stability; NANOHYBRIDS; EXTRACTION;
D O I
10.20964/2019.07.54
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
A highly sensitive electrode based on graphene oxide and functionalized multiwall carbon nanotube hybrid composite as coated on glassy carbon electrode (GCE) for the electrochemical rutin sensor. The as-prepared GO/f-MWCNTs@nafion composite was characterized by promising analysis such as field emission scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), Fourier transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS), UV-Vis Diffusive reflectance spectroscopy (UV-DRS). The GO/f-MWCNTs@nafion/GCE hybrid nanocomposite revealed substantial electrocatalytic activity toward the rutin sensor. The GO/f-MWCNTs@nafion/GCE electrode manifested voltammetric response over the concentration ranging of 0.02 to 39.69 mu M with a limit of detection (LOD) 0.004 nM, respectively. This analytical values suppressed the previously existing method for the electrochemical sensing of rutin. Additionally, the modified electrode proposed excellent stability, repeatability, and sensitivity.
引用
收藏
页码:6065 / 6076
页数:12
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