MCM-41-N-propylsulfamic acid: An efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphtols

被引：66
作者：
Hajjami, Maryam [1 ]
Ghorbani, Farshid [2 ]
Bakhti, Fariba [1 ]
机构：
[1] Ilam Univ, Fac Sci, Dept Chem, Ilam, Iran
[2] Univ Kurdistan, Fac Nat Resource, Dept Environm, Sanandaj 6677715177, Iran
来源：
APPLIED CATALYSIS A-GENERAL | 2014年 / 470卷
关键词：
1-Amidoalkyl-2-naphtols; MCM-41; MCM-41-N-propylsulfamic acid; Solvent-free; Multicomponent reaction; SOLVENT-FREE CONDITIONS; RECYCLABLE HETEROGENEOUS CATALYST; AMIDOALKYL NAPHTHOLS; MESOPOROUS SILICA; REUSABLE CATALYST; ROOM-TEMPERATURE; FACILE SYNTHESIS; TRITYL CHLORIDE; NEUTRAL MEDIA; BETA-NAPHTHOL;
D O I：
10.1016/j.apcata.2013.11.002
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
An efficient, one-pot three-component condensation of aromatic aldehydes, acetamide and 2-naphtol in the presence of catalytic amounts of MCM-41-N-propylsulfamic acid under thermal solvent-free conditions is described for the preparation of 1-amidoalkyl-2-naphtols in good to excellent yields. In this work, MCM-41-N-propylsulfamic acid was prepared by reaction of propylamine functionalized MCM-41 and chlorosulfonic acid and characterized by FTIR, XRD and TGA. (C) 2013 Elsevier B.V. All rights reserved.
引用
收藏
页码：303 / 310
页数：8
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