X-ray magnetic spectroscopy at high pressure: performance of SPring-8 BL39XU

被引:44
作者
Kawamura, Naomi [1 ]
Ishimatsu, Naoki [2 ]
Maruyama, Hiroshi [2 ]
机构
[1] Japan Synchrotron Radiat Res Inst SPring 8, Sayo, Hyogo 6795198, Japan
[2] Hiroshima Univ, Grad Sch Sci, Dept Phys Sci, Hiroshima 7398526, Japan
关键词
X-ray magnetic circular dichroism; multiple extreme conditions; high pressure; diamond anvil cell; in situ pressure calibration; Mn3GaC; ErCo2; FE72PT28 INVAR ALLOY; CIRCULAR-DICHROISM; PHASE-TRANSITION; RARE-EARTH; EDGE XMCD; MN3GAC; POLARIZATION; MOMENT; IRON;
D O I
10.1107/S0909049509034700
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An X-ray magnetic circular dichroism experiment under multiple extreme conditions, 2 <= T <= 300 K, H <= 10 T and P <= 50 GPa, has been achieved at SPring-8 BL39XU. A combination of the high-brilliant X-ray beam and a helicity-controlled technique enabled the dichroic signal to be recorded with high accuracy. The performance is shown by the outcome of pressure-induced ferromagnetism in Mn3GaC and the pressure-suppressed Co moment in ErCo2. Two technical developments, a tiny diamond anvil cell inserted into a superconducting magnet and in situ pressure calibration using 90 degrees Bragg diffraction from a NaCl marker, are also presented. X-ray magnetic spectroscopy under multiple extreme conditions is now opening a new approach to materials science.
引用
收藏
页码:730 / 736
页数:7
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