Nanocrystalline Fe-C composites obtained by mechanical alloying of iron and carbon nanotubes

被引:32
作者
Boshko, O. [1 ]
Nakonechna, O. [1 ]
Belyavina, N. [1 ]
Dashevskyi, M. [1 ]
Revo, S. [1 ]
机构
[1] Taras Shevchenko Natl Univ Kyiv, Dept Phys, 4 Glushkov Ave, UA-03022 Kiev, Ukraine
关键词
Composite materials; Powder metallurgy; Crystal structure; X-ray diffraction;
D O I
10.1016/j.apt.2016.12.026
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Mechanical alloying of the elemental powder mixture of iron and multiwalled carbon nanotubes (10, 20 and 30 vol.%) was performed in a high energy planetary ball mill. Nanocomposite materials obtained were examined by X-ray diffraction method as well as by transmission and scanning electron microscopy. It is shown that several phases were forming at the different stages of the milling process, namely, alpha-(Fe,C) and gamma-(Fe,C) supersaturated solid solutions along with the Fe3-xC and the Fe7C3 carbide phases. The hardness and magnetic properties (Curie temperature and coercive force) of the nanocomposite materials obtained were studied. The process of the mechanical alloying of materials studied has been analyzed. (C) 2017 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.
引用
收藏
页码:964 / 972
页数:9
相关论文
共 20 条
[1]   Nanocrystalline steel obtained by mechanical alloying of iron and graphite subsequently compacted by high-pressure torsion [J].
Borchers, Christine ;
Garve, Clemens ;
Tiegel, Marie ;
Deutges, Martin ;
Herz, Andreas ;
Edalati, Kaveh ;
Pippan, Reinhard ;
Horita, Zenji ;
Kirchheim, Reiner .
ACTA MATERIALIA, 2015, 97 :207-215
[2]   Effect of the carbon nanotubes on structure and magnetic properties of the Fe-Cu (4:1) composites [J].
Boshko, O. ;
Nakonechna, O. ;
Dashevskyi, M. ;
Ivanenko, R. ;
Belyavina, N. ;
Revo, S. .
ADVANCED POWDER TECHNOLOGY, 2016, 27 (04) :1101-1108
[3]   Nanocrystalline Fe-C alloys produced by ball milling of iron and graphite [J].
Chen, Y. Z. ;
Herz, A. ;
Li, Y. J. ;
Borchers, C. ;
Choi, P. ;
Raabe, D. ;
Kirchheim, R. .
ACTA MATERIALIA, 2013, 61 (09) :3172-3185
[4]   Grain-size dependence of coercive force in sputtered and annealed iron films [J].
Echigoya, J ;
Yue, R .
JOURNAL OF MATERIALS SCIENCE, 2005, 40 (12) :3209-3212
[5]   Microstructure characterization of nanocrystalline Fe3C synthesized by high-energy ball milling [J].
Ghosh, B. ;
Pradhan, S. K. .
JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 477 (1-2) :127-132
[6]   Transformation of carbon nanotubes to nanoparticles by ball milling process [J].
Li, YB ;
Wei, BQ ;
Liang, J ;
Yu, Q ;
Wu, DH .
CARBON, 1999, 37 (03) :493-497
[7]  
MAGER A, 1952, ANN PHYS-BERLIN, V11, P15
[8]   SOLID-STATE AMORPHIZATION OF FE-C ALLOY BY MECHANICAL ALLOYING [J].
NASU, T ;
NAGAOKA, K ;
ITOH, N ;
SUZUKI, K .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1990, 122 (02) :216-218
[9]  
Nowosielski R., 2005, MAT 13 INT SCI C ACH, P481
[10]  
NOWOSIELSKI R, 2006, J ACHIEV MAT MANUF E, V18, P167