COPPER(II) IONS MEDIATED CRYSTAL FORMATION OF 3-(3-HYDROXY PHENYL)-1-PHENYL-1H-PYRAZOLE-4-CARBALDEHYDE

被引：0
|
作者：
Banpurkar, Anita R. [1 ]
Wazalwar, Sach N. S. [1 ]
Perdih, Franc [2 ]
机构：
[1] Rajiv Gandhi Coll Engn Res & Technol, Dept Appl Chem, Chandrapur 442403, MS, India
[2] Univ Ljubljana, Fac Chem & Chem Technol, SI-1000 Ljubljana, Slovenia
来源：
BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2020年 / 34卷 / 03期
关键词：
Cu2+ assisted crystal growth; Pyrazole-4-carbaldehyde; X-ray crystal study; Hydrogen bonding study; BIOLOGICAL EVALUATION; MOLECULAR DOCKING; DESIGN; DERIVATIVES; PYRAZOLE; ANTICANCER; SAR;
D O I：
10.4314/bcse.v34i3.13
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Schiff base obtained from 3-hydroxyacetophenone and phenylhydrazine was subjected to Vilsmeier-Haack reaction to obtain 3-(3-hydroxyphenyl)-1-phenyl-1H-pyrazole-4-carbaldehyde (2). Successful formation of crystals of 2 was achieved using copper ions (Cu2+) as template. Present paper reports study of spectroscopic characterization and single-crystal X-ray study of 2. Hydrogen bonding network between 2 and water molecules enable the formation of 2D layer along ab-plane supported also by pi center dot center dot center dot pi stacking interactions of parallel molecules in head-to-head fashion.
引用
收藏
页码：589 / 596
页数：8
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