Formation of Ni57Zr20Ti22Pb1 amorphous powders by mechanical alloying

被引:0
作者
Lee, P. Y. [1 ]
Hung, S. S. [2 ]
Jang, Jason S. C. [2 ]
Chen, G. S. [3 ]
机构
[1] Natl Taiwan Ocean Univ, Inst Mat Engn, Chilung 202, Taiwan
[2] I Shou Univ, Dept Mat Sci & Engn, Kaohsiung 840, Taiwan
[3] Feng Chia Univ, Dept Mat Sci, Taichung 407, Taiwan
来源
THERMEC 2006, PTS 1-5 | 2007年 / 539-543卷
关键词
mechanical alloying; amorphous phase; supercooled liquid region; glass transition; Ni-based alloys;
D O I
10.4028/www.scientific.net/MSF.539-543.2767
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In the current study, the amorphization behavior of mechanically alloyed Ni57Zr20Ti22Pb1 powder was examined in details. The conventional X-ray diffraction results confirm that the fully amorphous powders formed after 5 hours of milling. The thermal stability of the Ni57Zr20Ti22Pb1 amorphous powders was investigated by differential scanning calorimeter (DSC). As the results demonstrated, the glass transition temperature (T-g) and the crystallization temperature (T-x) are 760 K and 850 K, respectively. The supercooled liquid region Delta T-x is 90 K. The appearance of wide supercooled liquid region may be mainly due to the Pb additions which cause the increasing differences in atomic size of mechanically alloyed Ni57Zr20Ti22Pb1 powders.
引用
收藏
页码:2767 / +
页数:3
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