Porous nano-structured micro-granules from silica-milk bi-colloidal suspension: Synthesis and characterization

被引：12

作者：

Biswas, Priyanka ^{[1
,5
]}

Sen, D. ^{[1
,5
]}

Mazumder, S. ^{[1
,5
]}

Melo, J. S. ^{[2
,5
]}

Basak, C. B. ^{[3
]}

Dasgupta, Kinshuk ^{[4
]}

机构：

[1] Bhabha Atom Res Ctr, Solid State Phys Div, Bombay 400085, Maharashtra, India

[2] Bhabha Atom Res Ctr, Nucl Agr & Biotechnol Div, Bombay 400085, Maharashtra, India

[3] Bhabha Atom Res Ctr, Glass & Adv Mat Div, Bombay 400085, Maharashtra, India

[4] Bhabha Atom Res Ctr, Mat Grp, Bombay 400085, Maharashtra, India

[5] Homi Bhabha Natl Inst, Bombay 400094, Maharashtra, India

来源：

COLLOIDS AND SURFACES B-BIOINTERFACES | 2017年 / 154卷

关键词：

Porous granules; Spray drying; Bi-colloids; SAXS; SANS; SEM; DRIED NANOCOMPOSITE POWDERS; FIELD-FLOW FRACTIONATION; MORPHOLOGICAL TRANSITION; MOLECULAR-SIEVES; NANOPARTICLES; SCATTERING; PARTICLES; DROPLETS; TEMPERATURE; DELIVERY;

D O I：

10.1016/j.colsurfb.2017.03.048

中图分类号：

Q6 [生物物理学];

学科分类号：

071011 ;

摘要：

Synthesis and characterization of nano-structured porous granules, with fairly defined morphology and porosity, is crucial because such granules are widely utilized for various technological applications. However, an easy, one-step, economic synthesis protocol for large scale production is extremely desirable. In the present work, we have reported the synthesis and characterization of the nano-structured micro granules using aerosol drying of bi-colloidal suspension of nano-silica and milk. Removal of soft organic component from the granules results in formation of meso and macro pores with moderate specific surface area. Granule morphology and porosity depends strongly on the concentration ratio of the individual components in the drying aerosol as well as the interaction between them. (C) 2017 Elsevier B.V. All rights reserved.

引用

页码：421 / 428

页数：8

共 61 条

[1] Porous Carriers for Controlled/Modulated Drug Delivery [J].

Ahuja, G. ;

Pathak, K. .

INDIAN JOURNAL OF PHARMACEUTICAL SCIENCES, 2009, 71 (06) :599-607

[2]

Aitchison J., 1957, The Lognormal Distribution

[3] Structuring adsorbents and catalysts by processing of porous powders [J].

Akhtar, Farid ;

Andersson, Linnea ;

Ogunwumi, Steven ;

Hedin, Niklas ;

Bergstrom, Lennart .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2014, 34 (07) :1643-1666

[4] Synthesis and optimization of colloidal silica nanoparticles and their functionalization with methacrylic acid [J].

Arantes, Tatiane M. ;

Pinto, Alexandre H. ;

Leite, Edson R. ;

Longo, Elson ;

Camargo, Emerson R. .

COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2012, 415 :209-217

[5]

Ardos A.B., 2013, FOOD SCI, V31, P99

[6] A review on solar cells from Si-single crystals to porous materials and quantum dots [J].

Badawy, Waheed A. .

JOURNAL OF ADVANCED RESEARCH, 2015, 6 (02) :123-132

[7] One-Step Fabrication of Thermally Stable TiO2/SiO2 Nanocomposite Microspheres by Evaporation-Induced Self-Assembly [J].

Bahadur, J. ;

Sen, D. ;

Mazumder, S. ;

Sastry, P. U. ;

Paul, B. ;

Bhatt, H. ;

Singh, S. G. .

LANGMUIR, 2012, 28 (31) :11343-11353

[8] Control of Buckling in Colloidal Droplets during Evaporation-Induced Assembly of Nanoparticles [J].

Bahadur, J. ;

Sen, D. ;

Mazumder, S. ;

Paul, B. ;

Bhatt, H. ;

Singh, S. G. .

LANGMUIR, 2012, 28 (03) :1914-1923

[9] Origin of Buckling Phenomenon during Drying of Micrometer-Sized Colloidal Droplets [J].

Bahadur, J. ;

Sen, D. ;

Mazumder, S. ;

Bhattacharya, S. ;

Frieinghaus, H. ;

Goerigk, G. .

LANGMUIR, 2011, 27 (13) :8404-8414

[10] Evaporation-induced self assembly of nanoparticles in non-buckling regime: Volume fraction dependent packing [J].

Bahadur, J. ;

Sen, D. ;

Mazumder, S. ;

Paul, Bhaskar ;

Khan, Arshad ;

Ghosh, G. .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2010, 351 (02) :357-364

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