Determination of Oxadiargyl Residues in Environmental Samples and Rice Samples

被引：28

作者：

Shi, Chenhui ^{[1
]}

Gui, Wenjun ^{[1
]}

Chen, Jie ^{[2
]}

Zhu, Guonian ^{[1
]}

机构：

[1] Zhejiang Univ, Inst Pesticide & Environm Toxicol, Hangzhou 310029, Zhejiang, Peoples R China

[2] Xixi Natl Wetland Pk, Hangzhou 310013, Zhejiang, Peoples R China

来源：

BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY | 2010年 / 84卷 / 02期

关键词：

Oxadiargyl; Residue; QuEChERS; Gas chromatography; MASS-SPECTROMETRIC DETECTION; FAST GAS-CHROMATOGRAPHY; LIQUID-CHROMATOGRAPHY; MULTIRESIDUE METHOD; PESTICIDE-RESIDUES;

D O I：

10.1007/s00128-009-9881-7

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Oxadiargyl is a commonly used herbicide in China. We developed a simple, fast, and high-throughput method employing gas chromatography with electron capture detector to determine oxadiargyl residues in food samples (rice, straws) and environmental samples (soil, water). Samples were prepared by a modified QuEChERS procedure. In this method, acetonitrile was used as the extracting solvent. The purifying step was omitted when the chromatographic conditions were optimized. Recoveries ranged from 82.9 to 112.0% for oxadiargyl in all samples, with relative standard deviation values lower than 6.2% at 0.01 mg/kg fortified concentration level.

引用

页码：236 / 239

页数：4

共 13 条

[11] Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection [J].

Paya, Paula ;

Anastassiades, Michelangelo ;

Mack, Dorothea ;

Sigalova, Irina ;

Tasdelen, Buenyamin ;

Oliva, Jose ;

Barba, Alberto .

ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2007, 389 (06) :1697-1714

[12]

Shi Chen-hui, 2008, Nongyaoxue Xuebao, V10, P349

[13]

TRACCHI G, 1997, 1997 BRIGHT CROP PRO

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