Determination of Oxadiargyl Residues in Environmental Samples and Rice Samples

被引：28
作者：
Shi, Chenhui [1 ]
Gui, Wenjun [1 ]
Chen, Jie [2 ]
Zhu, Guonian [1 ]
机构：
[1] Zhejiang Univ, Inst Pesticide & Environm Toxicol, Hangzhou 310029, Zhejiang, Peoples R China
[2] Xixi Natl Wetland Pk, Hangzhou 310013, Zhejiang, Peoples R China
来源：
BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY | 2010年 / 84卷 / 02期
关键词：
Oxadiargyl; Residue; QuEChERS; Gas chromatography; MASS-SPECTROMETRIC DETECTION; FAST GAS-CHROMATOGRAPHY; LIQUID-CHROMATOGRAPHY; MULTIRESIDUE METHOD; PESTICIDE-RESIDUES;
D O I：
10.1007/s00128-009-9881-7
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
Oxadiargyl is a commonly used herbicide in China. We developed a simple, fast, and high-throughput method employing gas chromatography with electron capture detector to determine oxadiargyl residues in food samples (rice, straws) and environmental samples (soil, water). Samples were prepared by a modified QuEChERS procedure. In this method, acetonitrile was used as the extracting solvent. The purifying step was omitted when the chromatographic conditions were optimized. Recoveries ranged from 82.9 to 112.0% for oxadiargyl in all samples, with relative standard deviation values lower than 6.2% at 0.01 mg/kg fortified concentration level.
引用
收藏
页码：236 / 239
页数：4
相关论文
共 13 条
  • [1] Anastassiades M, 2003, J AOAC INT, V86, P412
  • [2] *AOAC INT, 2006, AOAC TRAIN COURS SER
  • [3] Chen P., 1999, PESTICIDE, V38, P20
  • [4] DICKMANN R, 1997, 1997 BRIGHT CROP PRO
  • [5] DIEZ C, 2005, 11 M INSTR AN
  • [6] FROST PR, 2003, INT C CROP SCI TECHN
  • [7] Effects of oxadiargyl on direct-seeded rice and Echinochloa crus-galli under aerobic and anaerobic conditions
    Gitsopoulos, TK
    Froud-Williams, RJ
    [J]. WEED RESEARCH, 2004, 44 (04) : 329 - 334
  • [8] Practical fast gas chromatography:: methods, instrumentation and applications
    Korytár, P
    Janssen, HG
    Matisová, E
    Brinkman, UAT
    [J]. TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2002, 21 (9-10) : 558 - 572
  • [9] Lehotay SJ, 2005, J AOAC INT, V88, P595
  • [10] Fast gas chromatography and its use in trace analysis
    Matisová, E
    Dömötörová, M
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2003, 1000 (1-2) : 199 - 221
12