Synthesis, characterization, and antimicrobial activity of new benzoylthiourea ligands

被引：19

作者：

Kurt, Guelsah ^{[1
]}

Sevgi, Fatih ^{[2
]}

Mercimek, Bedrettin ^{[1
]}

机构：

[1] Selcuk Univ, Dept Chem, Fac Educ, TR-42099 Meram, Konya, Turkey

[2] Selcuk Univ, Vocat Sch Hlth Serv, TR-42003 Konya, Turkey

来源：

CHEMICAL PAPERS | 2009年 / 63卷 / 05期

关键词：

benzoylthiourea; antimicrobial activity; thermal properties; SEM; synthesis; CRYSTAL-STRUCTURE; THERMAL-BEHAVIOR; COMPLEXES; NI(II); PALLADIUM(II); DERIVATIVES; COPPER(II); RECOVERY; THIOUREA; CO(II);

D O I：

10.2478/s11696-009-0055-1

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In this study, new benzoylthiourea derivatives, (E)-N-[(2-benzamidomethyleneamino)ethylcarbamothioyl]benzamide H(3)L', N-(1-(3-benzoylthioureido)propan-2-ylcarbamothioyl)-benzamide H(4)LaEuro(3), (E)-N-[4-(benzamidomethyleneamino)phenylcarbamothioyl]benzamide H(3)LaEuro ', were synthesized. Structures of the compounds were identified by spectroscopic techniques. In addition, all synthesized compounds were evaluated for in vitro antibacterial and antifungal activity. Compound H(3)LaEuro ' exhibited antibacterial activity.

引用

页码：548 / 553

页数：6

共 18 条

[1] Benzoylthiourea-modified mesoporous silica for mercury(II) removal [J].

Antochshuk, V ;

Olkhovyk, O ;

Jaroniec, M ;

Park, IS ;

Ryoo, R .

LANGMUIR, 2003, 19 (07) :3031-3034

[2] Normal coordinate analysis and crystal structure of N,N-dimethyl-N′-(2-chloro-benzoyl)thiourea [J].

Arslan, Hakan ;

Kulcu, Nevzat ;

Floerke, Ulrich .

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2006, 64 (04) :1065-1071

[3]

Avsar G, 2003, TURK J CHEM, V27, P281

[4]

Avsar G, 2002, TURK J CHEM, V26, P607

[5]

BAUER AW, 1966, AM J CLIN PATHOL, V45, P493

[6] Synthesis, characterization and antimicrobial activities of transition metal complexes of N,N-dialkyl-N′-(2-chlorobenzoyl)thiourea derivatives [J].

Binzet, Gun ;

Arslan, Hakan ;

Floerke, Ulrich ;

Kuelcue, Nevzat ;

Duran, Nizami .

JOURNAL OF COORDINATION CHEMISTRY, 2006, 59 (12) :1395-1406

[7] Oxidative cyclization and coordinate polymerization of N-benzoyl-N′-(2-pyridyl) thiourea with copper(II) chloride [J].

Che, DJ ;

Li, G ;

Yu, Z ;

Zou, DP ;

Du, CX .

INORGANIC CHEMISTRY COMMUNICATIONS, 2000, 3 (10) :537-540

[8] N-benzoyl-N'-alkylthioureas and their complexes with Ni(II), Co(III) and Pt(II) -: crystal structure of 3-benzoyl-l-butyl-l-methyl-thiourea:: activity against fungi and yeast [J].

del Campo, R ;

Criado, JJ ;

Gheorghe, R ;

González, FJ ;

Hermosa, MR ;

Sanz, F ;

Manzano, JL ;

Monte, E ;

Rodríguez-Fernández, E .

JOURNAL OF INORGANIC BIOCHEMISTRY, 2004, 98 (08) :1307-1314

[9] Liquid-liquid extraction of palladium(II) and gold(III) with N-benzoyl-N′,N′-diethylthiourea and the synthesis of a palladium benzoylthiourea complex [J].

Domínguez, M ;

Anticó, E ;

Beyer, L ;

Aguirre, A ;

García-Granda, S ;

Salvadó, V .

POLYHEDRON, 2002, 21 (14-15) :1429-1437

[10] Selective. recovery and preconcentration of mercury with a benzoylthiourea-solid supported liquid membrane system [J].

Fontàs, C ;

Hidalgo, M ;

Salvadó, V ;

Anticó, E .

ANALYTICA CHIMICA ACTA, 2005, 547 (02) :255-261

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