Five-membered 2,3-dioxo heterocycles: LXVI. Reactions of (2Z,5Z)-1-aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones with o-phenylenediamine and hydrazine. Crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone

被引：3

作者：

Khalturina, V. V. ^{[1
]}

Shklyaev, Yu. V. ^{[1
]}

Aliev, Z. G. ^{[2
]}

Maslivets, A. N. ^{[3
]}

机构：

[1] Russian Acad Sci, Inst Tech Chem, Ural Div, Perm, Russia

[2] Russian Acad Sci, Inst Chem Phys Problems, Chernogolovka, Moscow Oblast, Russia

[3] Perm State Univ, Perm 614990, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2009年 / 45卷 / 10期

基金：

俄罗斯基础研究基金会;

关键词：

1,3,4,6-TETRACARBONYL COMPOUNDS;

D O I：

10.1134/S1070428009100169

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

(2Z,5Z)-1-Aryl-3-hydroxy-5-[3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]pent-2-ene-1,4-diones reacted with o-phenylenediamine and hydrazine to give 3-[(Z)-2-aryl-2-oxoethylidene]-1,2,3,4-tetrahydroquinoxalin-2-ones and 1-(3-aryl-1H-pyrazol-5-yl)-2-[(Z)-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]ethanones, respectively. The crystalline and molecular structure of 2-{(Z)-8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-(3-phenyl-1H-pyrazol-5-yl)ethanone was determined by X-ray analysis.

引用

页码：1519 / 1522

页数：4

共 9 条

[1] COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92
ALTOMARE, A
CASCARANO, G
GIACOVAZZO, C
GUAGLIARDI, A
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) : 343 - 350
[2] ANDREICHIKOV YS, 1982, KHIM GETEROTSIKL+, P420
[3] ANDREICHIKOV YS, 1978, ZH ORG KHIM+, V14, P169
[4] ANDREICHIKOV YS, 1978, KHIM GETEROTSIKL+, P407
[5] Five-membered 2,3-dioxo heterocycles: LXV. Reaction of 1-methyl-3,4-dihydroisoquinolines with aroylketenes. crystalline and molecular structure of (1Z,3Z)-4-hydroxy-1-[6,7-dimethoxy-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-4-phenylbut-3-en-2-one
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
[J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (10) : 1515 - 1518
[6] Five-membered 2,3-dioxoheterocycles: LXIV. Reactions of 1-methyl-3,4-dihydroisoquinolines with 5-arylfuran-2,3-diones and (Z)-alkyl 4-aryl-2-hydroxy-4-oxobut-2-enoates. Crystal and molecular structure of (2Z,5Z)-3-hydroxy-5-{8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-phenylpent-2-ene-1,4-dione
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
[J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (05) : 728 - 734
[7] 1,3,4,6-Tetracarbonyl compounds: V. Reaction of 1,6-disubstituted 3,4-dihydroxy-2,4-hexadiene-1,6-diones with 2,3-diaminopyridine
Koz'minykh, VO
Sof'ina, OA
Igidov, NM
Koz'minykh, EN
[J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2001, 37 (11) : 1649 - 1654
[8] Tetracarbonyl systems:: VII.: Reactions of 1,3,4,6-tetracarbonyl compounds with o-aminothiophenol in the synthesis of regioisomeric 3(2)-aroylmethylene-1,4-benzothiazin-2(3)ones
Kozminykh, VO
Igidov, NM
Kozminykh, EN
[J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2003, 39 (06) : 863 - 868
[9] Sheldrick GM., 1998, SHELX 97 PROGRAMS CR

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