Synthesis and characterization of a novel derivative of chitosan

被引：64
|
作者：
Ding, W
Lian, Q
Samuels, RJ
Polk, MB [1 ]
机构：
[1] Georgia Inst Technol, Sch Text & Fiber Engn, Atlanta, GA 30332 USA
[2] Georgia Inst Technol, Sch Chem Engn, Atlanta, GA 30332 USA
来源：
POLYMER | 2003年 / 44卷 / 03期
关键词：
chitosan-NLO graft-copolymer; polarized FTIR; NMR;
D O I：
10.1016/S0032-3861(02)00834-0
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
The graft-copolymer of chitosan with 4-(6-methacryloxyhexyloxy)-4'-nitrobiphenyl I was synthesized by radical polymerization. Graft-copolymerization was carried out under homogeneous conditions with AIBN as initiator and 2 wt% acetic acid as solvent. Homo-polymerization of I was also carried out to obtain material for comparative analysis. The resulting chitosan graft-copolymers were isolated, purified and characterized with FTIR, NMR, DSC, and TGA. Films were then prepared and characterized by X-ray diffraction, wave guide coupling and infrared dichroism techniques. (C) 2002 Published by Elsevier Science Ltd.
引用
收藏
页码：547 / 556
页数：10
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