Synthesis and antioxidant properties of bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite

被引：0

作者：

Akhmadullin, R. M. ^{[1
]}

Galiev, M. F. ^{[2
]}

Nugumanova, G. N. ^{[2
]}

Cherezova, E. N. ^{[2
]}

Gazizov, A. S. ^{[3
]}

Verizhnikov, L. V. ^{[1
]}

Akhmadullina, A. G. ^{[1
]}

Diachkov, I. M. ^{[2
]}

机构：

[1] R&D AhmadullinS Sci & Technol, Kazan 420015, Russia

[2] Kazan Natl Res Technol Univ, Kazan, Russia

[3] AE Arbuzov Inst Organ & Phys Chem, Kazan, Russia

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2021年 / 196卷 / 07期

关键词：

Bis(3-(3; 5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite; synthesis; antioxidant properties; IR; NMR spectroscopy; 2; 2-diphenyl-1-picrylhydrazyl; thermal oxidation;

D O I：

10.1080/10426507.2021.1885034

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite was synthesized by reaction of 2,6-di-tert-butyl-4-(3-hydroxyproyl)phenol with dibutyl phosphite. The structure of bis(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl)phosphite was supported by IR and NMR (H-1, C-13, P-31) spectroscopy; its composition was confirmed by elemental analysis. High antioxidant activity of the synthesized phosphite has been shown in a model reaction with the free chromogen-radical 2,2-diphenyl-1-picrylhydrazyl and under conditions of accelerated thermal oxidation of paraffinic and mineral oils.

引用

页码：643 / 646

页数：4

共 9 条

[1] Bondet V, 1997, FOOD SCI TECHNOL-LEB, V30, P609
[2] Havin Z.J., 1977, QUICK CHEM REFERENCE
[3] Krysin A.P., 1995, RU PATENT 1, V814
[4] Kuliev A. M., 1985, CHEM TECHNOLOGY OILS
[5] Abnormal solvent effects on hydrogen atom abstraction. 2. Resolution of the curcumin antioxidant controversy. The role of sequential proton loss electron transfer
Litwinienko, G
Ingold, KU
[J]. JOURNAL OF ORGANIC CHEMISTRY, 2004, 69 (18) : 5888 - 5896
[6] Maslova, 1981, CHEM TECHNOLOGY POLY
[7] Nugumanova G.N., 2009, POLYFUNCTIONAL STABI
[8] Carbonic anhydrase inhibitors. Inhibition of human erythrocyte isozymes I and II with a series of antioxidant phenols
Senturk, Murat
Gulcin, Ilhami
Dastan, Arif
Kufrevioglu, O. Irfan
Supuran, Claudiu T.
[J]. BIOORGANIC & MEDICINAL CHEMISTRY, 2009, 17 (08) : 3207 - 3211
[9] ZENKOV NK, 2003, PHENOLIC BIOANTIOXID

← 1 →