Quick gas chromatographic method for determining common pesticides in musts and wines

被引：18

作者：

Sala, C

Busto, O

Guasch, J

机构：

[1] GENERALITAT CATALUNYA,CERTA,UNITAT ENOL,TARRAGONA 43005,SPAIN

[2] UNIV ROVIRA & VIRGILI,ESCOLA ENOL TARRAGONA,DEPT QUIM,TARRAGONA 43005,SPAIN

来源：

CHROMATOGRAPHIA | 1997年 / 44卷 / 5-6期

关键词：

gas chromatography; wine analysis; pesticides;

D O I：

10.1007/BF02466401

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A rapid method based on gas chromatography which determines parathion-methyl, fenitrothion, chlorpyrifos, dichlofluanid, vinclozolin, chlozolinate, procymidone and iprodione is described. It involves quantitative extraction with n-hexane and determination by capillary gas chromatography using an electron capture detector. Pesticides were satisfactorily separated in 15 min with a phenylmethylsilicone fused-silica capillary column under isothermal conditions. Quantitation was carried out using dieldrin as internal standard. The method seems appropriate for oenological laboratory work because of its simplicity and rapidity. It was successfully used to identify and quantify pesticides studied in musts and wines.

引用

页码：320 / 324

页数：5

共 17 条

[1]

Bertrand A., 1990, Journal International des Sciences de la Vigne et du Vin, V24, P37

[2]

Bushway R. J., 1992, Food analysis by HPLC., P507

[3] MULTIRESIDUE METHOD FOR PESTICIDE DETERMINATION IN WINE BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

CABRAS, P ;

TUBEROSO, C ;

MELIS, M ;

MARTINI, MG .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1992, 40 (05) :817-819

[4] REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY OF PESTICIDES .7. ANALYSIS OF VINCLOZOLIN, IPRODIONE, PROCYMIDONE, DICHLOROLINATE AND THEIR DEGRADATION PRODUCT 3,5-DICHLOROANILINE ON WHITE MUST AND WINE EXTRACTS [J].

CABRAS, P ;

DIANA, P ;

MELONI, M ;

PIRISI, R ;

PIRISI, FM .

JOURNAL OF CHROMATOGRAPHY, 1983, 256 (01) :176-181

[5]

CANTAGREL R, 1993, FEUILLETS VERDS OIV, P939

[6]

FLORI P, 1990, VIGNEVINI, V31, P7

[7]

GARCIACAZORLA J, 1994, AM J ENOL VITICULT, V45, P338

[8] CHLOZOLINATE FATE DURING VINIFICATION PROCESS [J].

GENNARI, M ;

NEGRE, M ;

GERBI, V ;

RAIMONDO, E ;

MINATI, JL ;

GANDINI, A .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1992, 40 (05) :898-900

[9]

HOLLAND PT, 1994, J AOAC INT, V77, P79

[10]

*OIV, 1995, B OIV, V777, P932

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