1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate

被引：5

作者：

Pervez, Humayun ^{[2
]}

Yaqub, Muhammad ^{[2
]}

Manzoor, Nazia ^{[2
]}

Tahir, M. Nawaz ^{[1
]}

Iqbal, M. Saeed ^{[3
]}

机构：

[1] Univ Sargodha, Dept Phys, Sargodha, Pakistan

[2] Bahauddin Zakariya, Dept Chem, Multan 60800, Pakistan

[3] Govt Coll Univ, Dept Chem, Lahore, Pakistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809043633

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C16H13N5O3S center dot CH4O, the dihedral angle between the isatin unit and the 2-methylphenyl group is 41.81 (2)degrees and intramolecular N-H center dot center dot center dot O and N-H center dot center dot center dot N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N-H center dot center dot center dot O, O-H center dot center dot center dot S and C-H center dot center dot center dot O interactions.

引用

页码：O2858 / U1801

页数：10

共 9 条

[1] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS
BERNSTEIN, J
DAVIS, RE
SHIMONI, L
CHANG, NL
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) : 1555 - 1573
[2] Bruker, 2007, APEX2 SAINT
[3] Bruker, 2005, SADABS
[4] Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI [DOI 10.1107/S0021889812029111, DOI 10.1107/S0021889899006020]
[5] Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]
[6] (Z)-4-Hexyl-1-(5-nitro-2-oxo-2,3-dihydro-1H-indol-3-ylidene)thiosemicarbazide
Pervez, Humayun
Yaqub, Muhammad
Manzoor, Nazia
Tahir, M. Nawaz
Iqbal, M. Saeed
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2698 - U326
[7] Revenko M. D., 1994, Crystallography Reports, V39, P42
[8] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
[9] Structure validation in chemical crystallography
Spek, Anthony L.
[J]. ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 : 148 - 155

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