Simultaneous determination of low Z elements in barium borosilicate glass samples by in situ current normalized particle induced gamma-ray emission methods

被引：18
作者：
Chhillar, S. [1 ,2 ]
Acharya, R. [1 ]
Mishra, R. K. [3 ]
Kaushik, C. P. [3 ]
Pujari, P. K. [1 ]
机构：
[1] Bhabha Atom Res Ctr, Radiochem Div, Mumbai 400085, Maharashtra, India
[2] Homi Bhabha Natl Inst, Dept Atom Energy, Mumbai 400094, Maharashtra, India
[3] Bhabha Atom Res Ctr, Waste Management Div, Mumbai 400085, Maharashtra, India
来源：
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2017年 / 312卷 / 03期
关键词：
Barium borosilicate glass; Chemical characterization; Low Z elements; PIGE; In situ current normalization; Prompt gamma-ray spectrometry; STRUCTURAL ASPECTS; QUALITY-CONTROL; PIXE-PIGE; IMMOBILIZATION; THORIUM; YIELDS; PIXE/PIGE; MATRIX; WASTE;
D O I：
10.1007/s10967-017-5251-9
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Particle induced gamma-ray emission (PIGE) method using 4 MeV proton beam was utilized to analyze two types of barium borosilicate glass (BaBSG) samples for quantification of concentrations of low Z elements. The in situ current normalization method was applied in the analysis of eight samples containing varying concentration of F along with Si, B and Na. Charge normalized PIGE method was applied to determine concentrations of above low Z elements including Li and Al in samples having simulated nuclear waste from reprocessing of thoria spent fuel. Synthetic samples and NIST SRMs were used for method validation.
引用
收藏
页码：567 / 576
页数：10
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