Synthesis and crystal structure of 4-cyano-3-fluorophenyl-3-(4-hexoxy-3-methoxyphenyl)acrylic acid ester

被引：0

作者：

Ren, Rui ^{[1
]}

Zhang, Shu-Sheng ^{[1
]}

Li, Xue-Mei ^{[1
]}

Li, Qiang ^{[1
]}

机构：

[1] Qingdao Univ Sci & Technol, Coll Chem & Mol Engn, Qingdao 266042, Peoples R China

来源：

ASIAN JOURNAL OF CHEMISTRY | 2007年 / 19卷 / 02期

关键词：

synthesis; crystal structure; 4-cyano-3-fluorophenyl; 3-(4-hexoxy-3-methoxyphenyl)-acrylic acid ester;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In present study, 4-cyano-3-fluorophenyl-3-(4-hexoxy-3-methoxyphenyl)acrylic acid ester was synthesized through the esterification of 2-fluoro-4-hydroxybenzonitrile and 3-(4hexoxy-3-methoxyphenyl)acrylic acid ester (4-hydroxyfurelic acid) using N,N'-dicyclohexyl-carbodiimide (DCC) as esterifyirig agent. The structure of the this compound was characterized using IR and'H NMR spectra and X-ray crystallography. The compound crystallizes in the triclinic system, space group P-1, with cell dimensions of a = 7.461(2), b = 11.781(3) c = 13.801(4) angstrom, alpha = 96.153(4), beta = 93.117(4), gamma 100.1207(5)degrees, V = 1183.7(6) angstrom(3) and Z = 1.

引用

页码：1437 / 1442

页数：6

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