Mechanism of titanocene-mediated epoxide opening through homolytic substitution

被引:128
作者
Gansauer, Andreas
Barchuk, Andriy
Keller, Florian
Schmitt, Martin
Grimme, Stefan
Gerenkamp, Mareike
Mueck-Lichtenfeld, Christian
Daasbjerg, Kim
Svith, Heidi
机构
[1] Univ Bonn, Kekule Inst Organ Chem & Biochem, D-53121 Bonn, Germany
[2] Univ Munster, Inst Organ Chem, D-49149 Munster, Germany
[3] Univ Aarhus, Dept Chem, DK-8000 Aarhus C, Denmark
关键词
D O I
10.1021/ja067054e
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The mechanism of titanocene-mediated epoxide opening was studied by a combination of voltammetric, kinetic, computational, and synthetic methods. With the aid of electrochemical investigations the nature of a number of Ti(III) complexes in solution was established. In particular, the distribution of monomeric and dimeric Ti(III) species was found to be strongly affected by the exact steric conditions. The overall rate constants of the reductive epoxide opening were determined for the first time. These data were employed as the basis for computational studies of the structure and energies of the epoxide-titanocene complexes, the transition states of epoxide opening, and the beta-titanoxy radicals formed. The results obtained provide a structural basis for the understanding of the factors determining the regioselectivity of ring opening and match the experimentally determined values. By employing substituted titanocenes even more selective epoxide openings could be realized. Moreover, by properly adjusting the steric demands of the catalysts and the substrates the first examples of reversible epoxide openings were designed.
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页码:1359 / 1371
页数:13
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