Characterization of illuminated manuscripts by laboratory-made portable XRD and micro-XRD systems

被引：44
作者：
Duran, A. [1 ]
Perez-Rodriguez, J. L. [2 ]
Espejo, T. [3 ]
Franquelo, M. L. [2 ]
Castaing, J. [1 ]
Walter, P. [1 ]
机构：
[1] CNRS, UMR 171, C2RMF, F-75001 Paris, France
[2] Univ Seville, CSIC, Mat Sci Inst Seville, Seville 41092, Spain
[3] Univ Granada, Painting Dept, Fine Arts Fac, E-18071 Granada, Spain
来源：
ANALYTICAL AND BIOANALYTICAL CHEMISTRY | 2009年 / 395卷 / 07期
关键词：
Arabic manuscripts; XRD portable system; Laboratory-made mu-XRD system; Micro-Raman; Archeometry; CULTURAL-HERITAGE; RAMAN; PIGMENTS; IDENTIFICATION; DIFFRACTION; MICRODIFFRACTION; SPECTROMETRY; INSTRUMENT; FTIR;
D O I：
10.1007/s00216-009-2992-5
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Illuminated Arabic manuscripts have been studied, employing two laboratory-made X-ray diffraction (XRD) systems developed recently in the C2RMF laboratory. The validity of the A mu-XRD and XRD portable systems for the study of this type of artworks has been demonstrated. A common observation in all the analyses is the presence of calcite and rutile; also, hematite, goethite, cinnabar, brass, anatase and barite were detected in the various colours. Differences between the results obtained by both techniques due to acquisition mode are discussed. In addition, other techniques such as X-ray fluorescence (XRF) and micro-Raman were used for the complete characterization of the manuscripts.
引用
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页码：1997 / 2004
页数：8
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